C₂₇H₂₅NO₅

Base Information

Chemical Name:C₂₇H₂₅NO₅
CAS No.:1592683-39-0
Molecular Formula:C₂₇H₂₅NO₅
Molecular Weight:443.499
Hs Code.:

C<sub>27</sub>H<sub>25</sub>NO<sub>5</sub>

Synonyms:C₂₇H₂₅NO₅

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Chemical Property of C₂₇H₂₅NO₅

Chemical Property:

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Technology Process of C₂₇H₂₅NO₅

There total 4 articles about C₂₇H₂₅NO₅ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 50.0%

: 1592683-38-9
C₂₇H₂₆BrNO₅

: 1592683-39-0
C₂₇H₂₅NO₅

Guidance literature:: With di-tert-butyl(methyl)phosphonium tetrafluoroborate salt; palladium diacetate; potassium carbonate; In dimethyl sulfoxide; at 130 ℃; for 0.1h; Inert atmosphere; Microwave irradiation;
DOI:10.1016/j.bmcl.2014.02.066

Reference yield:

: 1592683-34-5
C₂₄H₂₂BrNO₄

: 1592683-39-0
C₂₇H₂₅NO₅

Guidance literature:: Multi-step reaction with 4 steps

1: pyridine; trifluorormethanesulfonic acid / dichloromethane / 0.5 h / -78 °C / Inert atmosphere

2: sodium tetrahydroborate / dichloromethane; methanol / 2.17 h / 0 °C

3: potassium carbonate / dichloromethane / 12 h / 20 °C

4: potassium carbonate; palladium diacetate; di-tert-butyl(methyl)phosphonium tetrafluoroborate salt / dimethyl sulfoxide / 0.1 h / 130 °C / Inert atmosphere; Microwave irradiation

With pyridine; sodium tetrahydroborate; trifluorormethanesulfonic acid; di-tert-butyl(methyl)phosphonium tetrafluoroborate salt; palladium diacetate; potassium carbonate; In methanol; dichloromethane; dimethyl sulfoxide; 1: |Bischler-Napieralski Reaction / 2: |Bischler-Napieralski Reaction;
DOI:10.1016/j.bmcl.2014.02.066

Reference yield:

: 1610775-08-0
C₂₄H₂₀BrNO₃

: 1592683-39-0
C₂₇H₂₅NO₅

Guidance literature:: Multi-step reaction with 3 steps

1: sodium tetrahydroborate / dichloromethane; methanol / 2.17 h / 0 °C

2: potassium carbonate / dichloromethane / 12 h / 20 °C

3: potassium carbonate; palladium diacetate; di-tert-butyl(methyl)phosphonium tetrafluoroborate salt / dimethyl sulfoxide / 0.1 h / 130 °C / Inert atmosphere; Microwave irradiation

With sodium tetrahydroborate; di-tert-butyl(methyl)phosphonium tetrafluoroborate salt; palladium diacetate; potassium carbonate; In methanol; dichloromethane; dimethyl sulfoxide; 1: |Bischler-Napieralski Reaction;
DOI:10.1016/j.bmcl.2014.02.066