C₃₁H₄₅ClO₈

Base Information

Chemical Name:C₃₁H₄₅ClO₈
CAS No.:943911-93-1
Molecular Formula:C₃₁H₄₅ClO₈
Molecular Weight:581.146
Hs Code.:

C<sub>31</sub>H<sub>45</sub>ClO<sub>8</sub>

Synonyms:C₃₁H₄₅ClO₈

Suppliers and Price of C₃₁H₄₅ClO₈

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of C₃₁H₄₅ClO₈

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of C₃₁H₄₅ClO₈

There total 11 articles about C₃₁H₄₅ClO₈ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 54812-37-2
2-iodo-1,3-dimethoxy-5-methylbenzene

: 943911-93-1
C₃₁H₄₅ClO₈

Guidance literature:: Multi-step reaction with 7 steps

1.1: 68 percent / sodium hydrogen carbonate; tetra-n-butylammonium iodide / Pd₂(dba)3CHCl₃ / dimethylsulfoxide / 96 h / 80 °C

2.1: 100 percent / NCS / acetonitrile / Heating

3.1: 65 percent / TiCl₄ / CH₂Cl₂ / 0 - 20 °C

4.1: 73 percent / BBr₃ / CH₂Cl₂ / -78 - 0 °C

5.1: 100 percent / DIPEA / 20 °C

6.1: 75 percent / PPTS / benzene

7.1: LHMDS; Ac₂O / tetrahydrofuran / -78 - 20 °C

7.2: Na/Hg; Na₂HPO₄ / methanol

With N-chloro-succinimide; pyridinium p-toluenesulfonate; acetic anhydride; boron tribromide; titanium tetrachloride; tetra-(n-butyl)ammonium iodide; sodium hydrogencarbonate; N-ethyl-N,N-diisopropylamine; lithium hexamethyldisilazane; tris(dibenzylideneacetone)dipalladium⁽⁰⁾ chloroform complex; In tetrahydrofuran; dichloromethane; dimethyl sulfoxide; acetonitrile; benzene; 7.1: Julia olefination;
DOI:10.1246/cl.2007.654

Reference yield:

: 78-79-5,9003-31-0
isoprene

: 943911-93-1
C₃₁H₄₅ClO₈

Guidance literature:: Multi-step reaction with 7 steps

1.1: 68 percent / sodium hydrogen carbonate; tetra-n-butylammonium iodide / Pd₂(dba)3CHCl₃ / dimethylsulfoxide / 96 h / 80 °C

2.1: 100 percent / NCS / acetonitrile / Heating

3.1: 65 percent / TiCl₄ / CH₂Cl₂ / 0 - 20 °C

4.1: 73 percent / BBr₃ / CH₂Cl₂ / -78 - 0 °C

5.1: 100 percent / DIPEA / 20 °C

6.1: 75 percent / PPTS / benzene

7.1: LHMDS; Ac₂O / tetrahydrofuran / -78 - 20 °C

7.2: Na/Hg; Na₂HPO₄ / methanol

With N-chloro-succinimide; pyridinium p-toluenesulfonate; acetic anhydride; boron tribromide; titanium tetrachloride; tetra-(n-butyl)ammonium iodide; sodium hydrogencarbonate; N-ethyl-N,N-diisopropylamine; lithium hexamethyldisilazane; tris(dibenzylideneacetone)dipalladium⁽⁰⁾ chloroform complex; In tetrahydrofuran; dichloromethane; dimethyl sulfoxide; acetonitrile; benzene; 7.1: Julia olefination;
DOI:10.1246/cl.2007.654

Reference yield:

: 943911-88-4
C₂₆H₃₃ClO₈S

: 943911-89-5
C₁₂H₂₀O₃

: 943911-93-1
C₃₁H₄₅ClO₈

Guidance literature:: C₂₆H₃₃ClO₈S; C₁₂H₂₀O₃; With acetic anhydride; lithium hexamethyldisilazane; In tetrahydrofuran; at -78 - 20 ℃;

With disodium hydrogenphosphate; sodium amalgam; In methanol; Further stages.;
DOI:10.1246/cl.2007.654