N,N-di-tert-butoxycarbonyl-9-(2,3,5-tri-O-benzoyl-α-L-arabinofuranosyl)adenine

Base Information

Chemical Name:N,N-di-tert-butoxycarbonyl-9-(2,3,5-tri-O-benzoyl-α-L-arabinofuranosyl)adenine
CAS No.:1311109-59-7
Molecular Formula:C₄₁H₄₁N₅O₁₁
Molecular Weight:779.803
Hs Code.:

Synonyms:N,N-di-tert-butoxycarbonyl-9-(2,3,5-tri-O-benzoyl-α-L-arabinofuranosyl)adenine

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Chemical Property of N,N-di-tert-butoxycarbonyl-9-(2,3,5-tri-O-benzoyl-α-L-arabinofuranosyl)adenine

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Technology Process of N,N-di-tert-butoxycarbonyl-9-(2,3,5-tri-O-benzoyl-α-L-arabinofuranosyl)adenine

There total 3 articles about N,N-di-tert-butoxycarbonyl-9-(2,3,5-tri-O-benzoyl-α-L-arabinofuranosyl)adenine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: 1311109-59-7
N,N-di-tert-butoxycarbonyl-9-(2,3,5-tri-O-benzoyl-α-L-arabinofuranosyl)adenine

Guidance literature:: With N-iodo-succinimide; trimethylsilyl trifluoromethanesulfonate; In dichloromethane; at -20 - 20 ℃; Molecular sieve; Inert atmosphere;

Reference yield: 80.0%

: 1311109-69-9
2,3,5-tri-O-benzoyl-α-L-arabinofuranosyl ortho-hexynylbenzoate

: 309947-86-2
N⁶,N⁶-bis(tert-butoxycarbonyl)adenine

: 1311109-59-7
N,N-di-tert-butoxycarbonyl-9-(2,3,5-tri-O-benzoyl-α-L-arabinofuranosyl)adenine

Guidance literature:: With [bis(trifluoromethanesulfonyl)imidate](triphenylphosphine)gold(I); In dichloromethane; at 20 ℃; Molecular sieve; Inert atmosphere;
DOI:10.1002/anie.201100514

Reference yield:

: 2,3,5-tri-O-benzoyl-α,β-L-arabinofuranose

: 1311109-59-7
N,N-di-tert-butoxycarbonyl-9-(2,3,5-tri-O-benzoyl-α-L-arabinofuranosyl)adenine

Guidance literature:: Multi-step reaction with 2 steps

1: dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine / dichloromethane / 3 h / 20 °C

2: [bis(trifluoromethanesulfonyl)imidate](triphenylphosphine)gold(I) / dichloromethane / 20 °C / Molecular sieve; Inert atmosphere

With dmap; [bis(trifluoromethanesulfonyl)imidate](triphenylphosphine)gold(I); 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine; In dichloromethane;
DOI:10.1002/anie.201100514