methyl [7-(benzyloxycarbonyl)amino-5,6,7-trideoxy-2,3-O-(isopropylidene)]-β-D-octaribofuranose

Base Information

Chemical Name:methyl [7-(benzyloxycarbonyl)amino-5,6,7-trideoxy-2,3-O-(isopropylidene)]-β-D-octaribofuranose
CAS No.:264622-12-0
Molecular Formula:C₂₀H₂₉NO₇
Molecular Weight:395.453
Hs Code.:

Synonyms:methyl [7-(benzyloxycarbonyl)amino-5,6,7-trideoxy-2,3-O-(isopropylidene)]-β-D-octaribofuranose

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Chemical Property of methyl [7-(benzyloxycarbonyl)amino-5,6,7-trideoxy-2,3-O-(isopropylidene)]-β-D-octaribofuranose

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Technology Process of methyl [7-(benzyloxycarbonyl)amino-5,6,7-trideoxy-2,3-O-(isopropylidene)]-β-D-octaribofuranose

There total 3 articles about methyl [7-(benzyloxycarbonyl)amino-5,6,7-trideoxy-2,3-O-(isopropylidene)]-β-D-octaribofuranose which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: methyl [7-(benzyloxycarbonyl)amino-5,6,7-trideoxy-2,3-O-(isopropylidene)-7-methoxycarbonyl]-β-D-heptaribofuranose

: 264622-12-0
methyl [7-(benzyloxycarbonyl)amino-5,6,7-trideoxy-2,3-O-(isopropylidene)]-β-D-octaribofuranose

Guidance literature:: With sodium tetrahydroborate; lithium chloride; In tetrahydrofuran; at 0 ℃; for 0.05h;

Reference yield:

: 21149-17-7
methyl 2-(benzyloxycarbonylamino)acrylate

: 264622-12-0
methyl [7-(benzyloxycarbonyl)amino-5,6,7-trideoxy-2,3-O-(isopropylidene)]-β-D-octaribofuranose

Guidance literature:: Multi-step reaction with 2 steps

1: 67 percent / CuI; Zn powder / tetrahydrofuran; H₂O

2: 85 percent / LiCl; NaBH₄ / tetrahydrofuran / 0.05 h / 0 °C

With sodium tetrahydroborate; copper(l) iodide; lithium chloride; zinc; In tetrahydrofuran; water; 1: Addition / 2: Reduction;

Reference yield:

: 38838-06-1
methyl 5-deoxy-5-iodo-2,3-isopropylidene-β-D-ribofuranoside

: 264622-12-0
methyl [7-(benzyloxycarbonyl)amino-5,6,7-trideoxy-2,3-O-(isopropylidene)]-β-D-octaribofuranose

Guidance literature:: Multi-step reaction with 2 steps

1: 67 percent / CuI; Zn powder / tetrahydrofuran; H₂O

2: 85 percent / LiCl; NaBH₄ / tetrahydrofuran / 0.05 h / 0 °C

With sodium tetrahydroborate; copper(l) iodide; lithium chloride; zinc; In tetrahydrofuran; water; 1: Addition / 2: Reduction;