rac-N-(1-benxyloxyallyl)-N-4-nitrobenzenesulfonyl-α-methyl-3,4-dimethoxyphenethylamine

Base Information

Chemical Name:rac-N-(1-benxyloxyallyl)-N-4-nitrobenzenesulfonyl-α-methyl-3,4-dimethoxyphenethylamine
CAS No.:859163-32-9
Molecular Formula:C₂₇H₃₀N₂O₇S
Molecular Weight:526.61
Hs Code.:

Synonyms:rac-N-(1-benxyloxyallyl)-N-4-nitrobenzenesulfonyl-α-methyl-3,4-dimethoxyphenethylamine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of rac-N-(1-benxyloxyallyl)-N-4-nitrobenzenesulfonyl-α-methyl-3,4-dimethoxyphenethylamine

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Technology Process of rac-N-(1-benxyloxyallyl)-N-4-nitrobenzenesulfonyl-α-methyl-3,4-dimethoxyphenethylamine

There total 4 articles about rac-N-(1-benxyloxyallyl)-N-4-nitrobenzenesulfonyl-α-methyl-3,4-dimethoxyphenethylamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 42.0%

: 859163-20-5
rac-N-4-nitrobenzenesulfonyl-α-methyl-3,4-dimethoxyphenethylamine

: 67515-49-5
1-benzyloxyallene

: 859163-32-9
rac-N-(1-benxyloxyallyl)-N-4-nitrobenzenesulfonyl-α-methyl-3,4-dimethoxyphenethylamine

Guidance literature:: With triethylamine; palladium diacetate; In acetonitrile; at 20 ℃; for 6h;
DOI:10.1021/jo050503t

Reference yield:

: 122-47-4
1-(3,4-dimethoxyphenyl)-2-nitropropene

: 859163-32-9
rac-N-(1-benxyloxyallyl)-N-4-nitrobenzenesulfonyl-α-methyl-3,4-dimethoxyphenethylamine

Guidance literature:: Multi-step reaction with 3 steps

1: 9.4 g / LiAlH₄ / tetrahydrofuran / 3 h / Heating

2: 55 percent / Et₃N / CH₂Cl₂ / 6 h / 20 °C

3: 42 percent / Et₃N / Pd(OAc)2 / acetonitrile / 6 h / 20 °C

With lithium aluminium tetrahydride; triethylamine; palladium diacetate; In tetrahydrofuran; dichloromethane; acetonitrile;
DOI:10.1021/jo050503t

Reference yield:

: 120-26-3
2-(3,4-dimethoxyphenyl)-1-methylethylamine

: 859163-32-9
rac-N-(1-benxyloxyallyl)-N-4-nitrobenzenesulfonyl-α-methyl-3,4-dimethoxyphenethylamine

Guidance literature:: Multi-step reaction with 2 steps

1: 55 percent / Et₃N / CH₂Cl₂ / 6 h / 20 °C

2: 42 percent / Et₃N / Pd(OAc)2 / acetonitrile / 6 h / 20 °C

With triethylamine; palladium diacetate; In dichloromethane; acetonitrile;
DOI:10.1021/jo050503t