C₃₁H₃₀O₆

Base Information

Chemical Name:C₃₁H₃₀O₆
CAS No.:1394902-94-3
Molecular Formula:C₃₁H₃₀O₆
Molecular Weight:498.576
Hs Code.:

C<sub>31</sub>H<sub>30</sub>O<sub>6</sub>

Synonyms:C₃₁H₃₀O₆

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Chemical Property of C₃₁H₃₀O₆

Chemical Property:

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Technology Process of C₃₁H₃₀O₆

There total 8 articles about C₃₁H₃₀O₆ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₃₇H₄₂O₈

: 1394902-94-3
C₃₁H₃₀O₆

Guidance literature:: With hydrogenchloride; In tetrahydrofuran; at 20 ℃; for 16h;
DOI:10.1021/ol302132s

Reference yield:

: 1394902-93-2
C₁₆H₂₅BO₅

: 1394902-94-3
C₃₁H₃₀O₆

Guidance literature:: Multi-step reaction with 3 steps

1: tetrakis(triphenylphosphine) palladium⁽⁰⁾; sodium carbonate / ethanol; water; toluene / 16 h / 105 °C / Inert atmosphere

2: 5% Pd/C; triethylamine; hydrogen / ethyl acetate / 24 h / 2250.23 Torr

3: hydrogenchloride / tetrahydrofuran / 16 h / 20 °C

With hydrogenchloride; tetrakis(triphenylphosphine) palladium⁽⁰⁾; 5% Pd/C; hydrogen; sodium carbonate; triethylamine; In tetrahydrofuran; ethanol; water; ethyl acetate; toluene; 1: |Suzuki-Miyaura Coupling;
DOI:10.1021/ol302132s

Reference yield:

: C₉H₁₁BrO₃

: 1394902-94-3
C₃₁H₃₀O₆

Guidance literature:: Multi-step reaction with 7 steps

1.1: potassium carbonate / acetone / 3 h / Inert atmosphere; Reflux

2.1: n-butyllithium / hexane; tetrahydrofuran / 0.5 h / -78 °C / Inert atmosphere

2.2: 2 h / -78 - 20 °C

3.1: potassium dihydrogenphosphate / water; diethyl ether / Inert atmosphere

4.1: magnesium sulfate / dichloromethane; water / 12 h / 20 °C / Inert atmosphere

5.1: tetrakis(triphenylphosphine) palladium⁽⁰⁾; sodium carbonate / ethanol; water; toluene / 16 h / 105 °C / Inert atmosphere

6.1: 5% Pd/C; triethylamine; hydrogen / ethyl acetate / 24 h / 2250.23 Torr

7.1: hydrogenchloride / tetrahydrofuran / 16 h / 20 °C

With hydrogenchloride; potassium dihydrogenphosphate; tetrakis(triphenylphosphine) palladium⁽⁰⁾; n-butyllithium; 5% Pd/C; hydrogen; sodium carbonate; magnesium sulfate; potassium carbonate; triethylamine; In tetrahydrofuran; diethyl ether; ethanol; hexane; dichloromethane; water; ethyl acetate; acetone; toluene; 5.1: |Suzuki-Miyaura Coupling;
DOI:10.1021/ol302132s