mycosporin-2 open form

Base Information

• Chemical Name: mycosporin-2 open form
• CAS No.: 77101-66-7
• Molecular Formula: C₁₃H₂₁NO₇
• Molecular Weight: 303.312

Synonyms:mycosporin-2 open form

Chemical Property of mycosporin-2 open form

Chemical Property:

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Technology Process of mycosporin-2 open form

There total 3 articles about mycosporin-2 open form which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

9-O-glucosylmycosporin-2 ring form → D-Glucose (2280-44-6) + mycosporin-2 ring form (63720-26-3) + mycosporin-2 open form (77101-66-7) + 9-O-glucosylmycosporin-2 open form

Guidance literature:

With hydrogenchloride; at 100 ℃; for 0.1h; Product distribution; var. times;

DOI:10.1016/0031-9422(81)85272-7

Reference yield:

4-(5-Hydroxy-5-hydroxymethyl-2-methoxy-3-oxo-cyclohex-1-enylamino)-5-((2R,3S,4R,5R,6S)-4,5,6-trihydroxy-2-hydroxymethyl-tetrahydro-pyran-3-yloxy)-pentanoic acid amide → alpha-D-glucopyranose (492-62-6) + mycosporine glutaminol (85769-64-8) + mycosporin-2 open form (77101-66-7) + 4-(5-Hydroxy-5-hydroxymethyl-2-methoxy-3-oxo-cyclohex-1-enylamino)-5-((2R,3S,4R,5R,6S)-4,5,6-trihydroxy-2-hydroxymethyl-tetrahydro-pyran-3-yloxy)-pentanoic acid

Guidance literature:

With hydrogenchloride; at 100 ℃; for 1.5h;

DOI:10.1016/S0040-4039(00)81328-3

Reference yield:

mycosporin-2 ring form (63720-26-3) → mycosporin-2 open form (77101-66-7)

Guidance literature:

With hydrogen cation;

DOI:10.1016/0031-9422(81)85273-9

upstream raw materials:

mycosporin-2 ring form

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