3-Methyl-2-methylsulfanyl-4-phenyl-4,5-dihydro-3H-benzo[d][1,3]diazepine; hydriodide

Base Information

Chemical Name:3-Methyl-2-methylsulfanyl-4-phenyl-4,5-dihydro-3H-benzo[d][1,3]diazepine; hydriodide
CAS No.:88057-55-0
Molecular Formula:C₁₇H₁₈N₂S*HI
Molecular Weight:410.322
Hs Code.:

Synonyms:3-Methyl-2-methylsulfanyl-4-phenyl-4,5-dihydro-3H-benzo[d][1,3]diazepine; hydriodide

Suppliers and Price of 3-Methyl-2-methylsulfanyl-4-phenyl-4,5-dihydro-3H-benzo[d][1,3]diazepine; hydriodide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 3-Methyl-2-methylsulfanyl-4-phenyl-4,5-dihydro-3H-benzo[d][1,3]diazepine; hydriodide

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 3-Methyl-2-methylsulfanyl-4-phenyl-4,5-dihydro-3H-benzo[d][1,3]diazepine; hydriodide

There total 2 articles about 3-Methyl-2-methylsulfanyl-4-phenyl-4,5-dihydro-3H-benzo[d][1,3]diazepine; hydriodide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 88057-54-9
3-Methyl-4-phenyl-1,3,4,5-tetrahydro-benzo[d][1,3]diazepine-2-thione

: 74-88-4
methyl iodide

: 88057-55-0
3-Methyl-2-methylsulfanyl-4-phenyl-4,5-dihydro-3H-benzo[d][1,3]diazepine; hydriodide

Guidance literature:: In 2-methoxy-ethanol; Ambient temperature;
DOI:10.1021/jm00369a029

Reference yield:

: 88057-41-4
(+/-)-2-amino-N-methyl-α-phenylbenzenethanamine

: 88057-55-0
3-Methyl-2-methylsulfanyl-4-phenyl-4,5-dihydro-3H-benzo[d][1,3]diazepine; hydriodide

Guidance literature:: Multi-step reaction with 2 steps

1: 52 percent / concd HCl / aq. ethanol / 1.) 60 deg C, 1 h, 2.) reflux, 24 h

2: 92 percent / 2-methoxy-ethanol / Ambient temperature

With hydrogenchloride; In ethanol; 2-methoxy-ethanol;
DOI:10.1021/jm00369a029