1-(4-(dec-9-enyl)-5-(2-ethylhexyl)-6-(4-methoxybenzyloxy)pyrimidin-2-yl)-3-(2,6-diisopropylphenyl)urea

Base Information

Chemical Name:1-(4-(dec-9-enyl)-5-(2-ethylhexyl)-6-(4-methoxybenzyloxy)pyrimidin-2-yl)-3-(2,6-diisopropylphenyl)urea
CAS No.:1422728-83-3
Molecular Formula:C₄₃H₆₄N₄O₃
Molecular Weight:685.006
Hs Code.:

Synonyms:1-(4-(dec-9-enyl)-5-(2-ethylhexyl)-6-(4-methoxybenzyloxy)pyrimidin-2-yl)-3-(2,6-diisopropylphenyl)urea

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Chemical Property of 1-(4-(dec-9-enyl)-5-(2-ethylhexyl)-6-(4-methoxybenzyloxy)pyrimidin-2-yl)-3-(2,6-diisopropylphenyl)urea

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Technology Process of 1-(4-(dec-9-enyl)-5-(2-ethylhexyl)-6-(4-methoxybenzyloxy)pyrimidin-2-yl)-3-(2,6-diisopropylphenyl)urea

There total 5 articles about 1-(4-(dec-9-enyl)-5-(2-ethylhexyl)-6-(4-methoxybenzyloxy)pyrimidin-2-yl)-3-(2,6-diisopropylphenyl)urea which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 1422728-82-2
1-(6-(dec-9-enyl)-5-(2-ethylhexyl)-4-oxo-1,4-dihydropyrimidin-2-yl)-3-(2,6-diisopropylphenyl)urea

: 824-94-2
p-methoxybenzyl chloride

: 1422728-83-3
1-(4-(dec-9-enyl)-5-(2-ethylhexyl)-6-(4-methoxybenzyloxy)pyrimidin-2-yl)-3-(2,6-diisopropylphenyl)urea

Guidance literature:: With potassium carbonate; In N,N-dimethyl-formamide; at 20 ℃; for 48h;
DOI:10.1002/anie.201204840

Reference yield:

: 1443253-63-1
C₂₃H₄₂O₃

: 1422728-83-3
1-(4-(dec-9-enyl)-5-(2-ethylhexyl)-6-(4-methoxybenzyloxy)pyrimidin-2-yl)-3-(2,6-diisopropylphenyl)urea

Guidance literature:: Multi-step reaction with 3 steps

1: ethanol / 24 h / Reflux

2: pyridine / 20 °C

3: potassium carbonate / N,N-dimethyl-formamide / 48 h / 20 °C

With pyridine; potassium carbonate; In ethanol; N,N-dimethyl-formamide;
DOI:10.1002/anie.201204840

Reference yield:

: 89359-54-6
9-bromo-1-nonene

: 1422728-83-3
1-(4-(dec-9-enyl)-5-(2-ethylhexyl)-6-(4-methoxybenzyloxy)pyrimidin-2-yl)-3-(2,6-diisopropylphenyl)urea

Guidance literature:: Multi-step reaction with 5 steps

1.1: sodium hydride / tetrahydrofuran / 0 °C

1.2: 0.5 h / -78 °C

1.3: -78 - 20 °C

2.1: potassium carbonate / N,N-dimethyl-formamide / 24 h / 70 °C

3.1: ethanol / 24 h / Reflux

4.1: pyridine / 20 °C

5.1: potassium carbonate / N,N-dimethyl-formamide / 48 h / 20 °C

With pyridine; sodium hydride; potassium carbonate; In tetrahydrofuran; ethanol; N,N-dimethyl-formamide;
DOI:10.1002/anie.201204840