N--(S)-α-methylbenzylamine

Base Information

• Chemical Name: N--(S)-α-methylbenzylamine
• CAS No.: 17430-32-9
• Molecular Formula: C₂₅H₂₆N₂O₃
• Molecular Weight: 402.493

Synonyms:N--(S)-α-methylbenzylamine

Chemical Property of N--(S)-α-methylbenzylamine

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Technology Process of N--(S)-α-methylbenzylamine

There total 11 articles about N--(S)-α-methylbenzylamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.0%

(S)-1-phenyl-ethylamine (2627-86-3) + N-Cbz-L-Phe (1161-13-3) → N--(S)-α-methylbenzylamine (17430-32-9)

Guidance literature:

With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In dichloromethane; at 20 ℃;

DOI:10.1039/b108735p

Reference yield:

(S)-1-phenyl-ethylamine (2627-86-3) + Cbz-Phe-OCH2CONH2 (4816-89-1) → N-Cbz-L-Phe (1161-13-3) + N--(S)-α-methylbenzylamine (17430-32-9)

Guidance literature:

With α-chymotrypsin immobilised on Celite; triethylamine; In acetonitrile; at 30 ℃; for 2h; pH=7.8;

DOI:10.1039/b108735p

Reference yield:

(S)-1-phenyl-ethylamine (2627-86-3) + 2,2,2-trifluoroethyl ((benzyloxy)carbonyl)-L-phenylalaninate (126028-14-6) → N-Cbz-L-Phe (1161-13-3) + N--(S)-α-methylbenzylamine (17430-32-9)

Guidance literature:

With α-chymotrypsin immobilised on Celite; triethylamine; In acetonitrile; at 30 ℃; for 5h; pH=7.8;

DOI:10.1039/b108735p

upstream raw materials:

(S)-1-phenyl-ethylamine

N-Cbz-L-Phe

Cbz-Phe-OCH₂CONH₂

2,2,2-trifluoroethyl ((benzyloxy)carbonyl)-L-phenylalaninate

Downstream raw materials:

(S)-2-Amino-3-phenyl-N-((S)-1-phenyl-ethyl)-propionamide

2-N-methylamino-1--3-phenylpropane

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