(E)-4-(1-ethynyl-1,5,9-trimethyldeca-4,8-dienyloxy)-6-methoxymethoxy-2-[2-(4-methoxymethoxyphenyl)ethyl]-2,3-dihydro-isoindol-1-one

Base Information

Chemical Name:(E)-4-(1-ethynyl-1,5,9-trimethyldeca-4,8-dienyloxy)-6-methoxymethoxy-2-[2-(4-methoxymethoxyphenyl)ethyl]-2,3-dihydro-isoindol-1-one
CAS No.:1425861-20-6
Molecular Formula:C₃₅H₄₅NO₆
Molecular Weight:575.745
Hs Code.:

Synonyms:(E)-4-(1-ethynyl-1,5,9-trimethyldeca-4,8-dienyloxy)-6-methoxymethoxy-2-[2-(4-methoxymethoxyphenyl)ethyl]-2,3-dihydro-isoindol-1-one

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Chemical Property of (E)-4-(1-ethynyl-1,5,9-trimethyldeca-4,8-dienyloxy)-6-methoxymethoxy-2-[2-(4-methoxymethoxyphenyl)ethyl]-2,3-dihydro-isoindol-1-one

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Technology Process of (E)-4-(1-ethynyl-1,5,9-trimethyldeca-4,8-dienyloxy)-6-methoxymethoxy-2-[2-(4-methoxymethoxyphenyl)ethyl]-2,3-dihydro-isoindol-1-one

There total 8 articles about (E)-4-(1-ethynyl-1,5,9-trimethyldeca-4,8-dienyloxy)-6-methoxymethoxy-2-[2-(4-methoxymethoxyphenyl)ethyl]-2,3-dihydro-isoindol-1-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 19894-78-1
(E)-2-acetyl-5,9-dimethyldeca-4,8-dienoic acid ethyl ester

: 1425861-20-6
(E)-4-(1-ethynyl-1,5,9-trimethyldeca-4,8-dienyloxy)-6-methoxymethoxy-2-[2-(4-methoxymethoxyphenyl)ethyl]-2,3-dihydro-isoindol-1-one

Guidance literature:: Multi-step reaction with 3 steps

1.1: sodium hydroxide / water; ethanol / 3 h / Reflux

2.1: tetrahydrofuran / 12 h / 20 °C

2.2: 3 h / 20 °C

3.1: potassium carbonate; potassium iodide; copper(l) iodide / acetone / 48 h / Reflux

With copper(l) iodide; potassium carbonate; potassium iodide; sodium hydroxide; In tetrahydrofuran; ethanol; water; acetone;
DOI:10.1055/s-0032-1317528

Reference yield:

: 16849-78-8
2-formyl-3,5-dihydroxybenzoic acid methyl ester

: 1425861-20-6
(E)-4-(1-ethynyl-1,5,9-trimethyldeca-4,8-dienyloxy)-6-methoxymethoxy-2-[2-(4-methoxymethoxyphenyl)ethyl]-2,3-dihydro-isoindol-1-one

Guidance literature:: Multi-step reaction with 3 steps

1.1: potassium carbonate / acetone / 12 h / 20 °C

2.1: methanol / 1 h

2.2: 0 - 20 °C

3.1: potassium carbonate; potassium iodide; copper(l) iodide / acetone / 48 h / Reflux

With copper(l) iodide; potassium carbonate; potassium iodide; In methanol; acetone;
DOI:10.1055/s-0032-1317528

Reference yield:

: 6138-90-5
trans-geranyl bromide

: 1425861-20-6
(E)-4-(1-ethynyl-1,5,9-trimethyldeca-4,8-dienyloxy)-6-methoxymethoxy-2-[2-(4-methoxymethoxyphenyl)ethyl]-2,3-dihydro-isoindol-1-one

Guidance literature:: Multi-step reaction with 4 steps

1.1: sodium hydride / tetrahydrofuran / 0.25 h / 0 °C

1.2: 12 h / 20 °C

2.1: sodium hydroxide / water; ethanol / 3 h / Reflux

3.1: tetrahydrofuran / 12 h / 20 °C

3.2: 3 h / 20 °C

4.1: potassium carbonate; potassium iodide; copper(l) iodide / acetone / 48 h / Reflux

With copper(l) iodide; sodium hydride; potassium carbonate; potassium iodide; sodium hydroxide; In tetrahydrofuran; ethanol; water; acetone;
DOI:10.1055/s-0032-1317528