6-methoxymethoxy-2-[2-(4-methoxymethoxyphenyl)ethyl]-4-((E)-1,5,9-trimethyl-1-vinyldeca-4,8-dienyloxy)-2,3-dihydroisoindol-1-one

Base Information

Chemical Name:6-methoxymethoxy-2-[2-(4-methoxymethoxyphenyl)ethyl]-4-((E)-1,5,9-trimethyl-1-vinyldeca-4,8-dienyloxy)-2,3-dihydroisoindol-1-one
CAS No.:1445069-48-6
Molecular Formula:C₃₅H₄₇NO₆
Molecular Weight:577.761
Hs Code.:

Synonyms:6-methoxymethoxy-2-[2-(4-methoxymethoxyphenyl)ethyl]-4-((E)-1,5,9-trimethyl-1-vinyldeca-4,8-dienyloxy)-2,3-dihydroisoindol-1-one

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Chemical Property of 6-methoxymethoxy-2-[2-(4-methoxymethoxyphenyl)ethyl]-4-((E)-1,5,9-trimethyl-1-vinyldeca-4,8-dienyloxy)-2,3-dihydroisoindol-1-one

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Technology Process of 6-methoxymethoxy-2-[2-(4-methoxymethoxyphenyl)ethyl]-4-((E)-1,5,9-trimethyl-1-vinyldeca-4,8-dienyloxy)-2,3-dihydroisoindol-1-one

There total 3 articles about 6-methoxymethoxy-2-[2-(4-methoxymethoxyphenyl)ethyl]-4-((E)-1,5,9-trimethyl-1-vinyldeca-4,8-dienyloxy)-2,3-dihydroisoindol-1-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 1425861-20-6
(E)-4-(1-ethynyl-1,5,9-trimethyldeca-4,8-dienyloxy)-6-methoxymethoxy-2-[2-(4-methoxymethoxyphenyl)ethyl]-2,3-dihydro-isoindol-1-one

: 1445069-48-6
6-methoxymethoxy-2-[2-(4-methoxymethoxyphenyl)ethyl]-4-((E)-1,5,9-trimethyl-1-vinyldeca-4,8-dienyloxy)-2,3-dihydroisoindol-1-one

Guidance literature:: With hydrogen; In ethyl acetate; at 20 ℃; for 6h; under 760.051 Torr;
DOI:10.1021/jo401116r

Reference yield:

: 1425861-04-6
4-hydroxy-6-methoxymethoxy-2-[2-(4-methoxymethoxyphenyl)ethyl]-2,3-dihydro-isoindol-1-one

: 1445069-48-6
6-methoxymethoxy-2-[2-(4-methoxymethoxyphenyl)ethyl]-4-((E)-1,5,9-trimethyl-1-vinyldeca-4,8-dienyloxy)-2,3-dihydroisoindol-1-one

Guidance literature:: Multi-step reaction with 2 steps

1: potassium carbonate; potassium iodide; copper(l) iodide / acetone / 48 h / Reflux

2: hydrogen / ethyl acetate / 6 h / 20 °C / 760.05 Torr

With copper(l) iodide; hydrogen; potassium carbonate; potassium iodide; In ethyl acetate; acetone;
DOI:10.1021/jo401116r

Reference yield:

: 1425861-17-1
(E)-carbonic acid 1-ethynyl-1,5,9-trimethyldeca-4,8-dienyl ester methyl ester

: 1445069-48-6
6-methoxymethoxy-2-[2-(4-methoxymethoxyphenyl)ethyl]-4-((E)-1,5,9-trimethyl-1-vinyldeca-4,8-dienyloxy)-2,3-dihydroisoindol-1-one

Guidance literature:: Multi-step reaction with 2 steps

1: potassium carbonate; potassium iodide; copper(l) iodide / acetone / 48 h / Reflux

2: hydrogen / ethyl acetate / 6 h / 20 °C / 760.05 Torr

With copper(l) iodide; hydrogen; potassium carbonate; potassium iodide; In ethyl acetate; acetone;
DOI:10.1021/jo401116r