(4R,5S)-4-(4-methylthiophenyl)-5-phenyloxycarbonyloxymethyl-2-oxazolidinone

Base Information

Chemical Name:(4R,5S)-4-(4-methylthiophenyl)-5-phenyloxycarbonyloxymethyl-2-oxazolidinone
CAS No.:909767-32-4
Molecular Formula:C₁₈H₁₇NO₅S
Molecular Weight:359.403
Hs Code.:

Synonyms:(4R,5S)-4-(4-methylthiophenyl)-5-phenyloxycarbonyloxymethyl-2-oxazolidinone

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Chemical Property of (4R,5S)-4-(4-methylthiophenyl)-5-phenyloxycarbonyloxymethyl-2-oxazolidinone

Chemical Property:

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Technology Process of (4R,5S)-4-(4-methylthiophenyl)-5-phenyloxycarbonyloxymethyl-2-oxazolidinone

There total 5 articles about (4R,5S)-4-(4-methylthiophenyl)-5-phenyloxycarbonyloxymethyl-2-oxazolidinone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.0%

: 909767-31-3
(2S,3R)-3-azido-1,2-diphenyloxycarbonyloxy-3-(4-methylthiophenyl)-propane

: 909767-32-4
(4R,5S)-4-(4-methylthiophenyl)-5-phenyloxycarbonyloxymethyl-2-oxazolidinone

Guidance literature:: With triphenylphosphine; In tetrahydrofuran; at 50 ℃; for 1h;
DOI:10.1016/j.tetasy.2006.06.009

Reference yield:

: 909767-29-9
(2R,3S)-2,3-epoxy-3-(4-methylthiophenyl)-1-propanol

: 909767-32-4
(4R,5S)-4-(4-methylthiophenyl)-5-phenyloxycarbonyloxymethyl-2-oxazolidinone

Guidance literature:: Multi-step reaction with 3 steps

1: 94 percent / sodium azide; ammonium chloride / H₂O; 2-methoxy-ethanol / 3 h / 100 °C

2: 90 percent / pyridine / CH₂Cl₂ / cooling

3: 71 percent / triphenylphosphine / tetrahydrofuran / 1 h / 50 °C

With pyridine; sodium azide; ammonium chloride; triphenylphosphine; In tetrahydrofuran; dichloromethane; 2-methoxy-ethanol; water;
DOI:10.1016/j.tetasy.2006.06.009

Reference yield:

: 906548-44-5
(1S,2S)-(+)-2-(dimethylamino)-1-[4-(methylthio)phenyl]propane-1,3-diol

: 909767-32-4
(4R,5S)-4-(4-methylthiophenyl)-5-phenyloxycarbonyloxymethyl-2-oxazolidinone

Guidance literature:: Multi-step reaction with 5 steps

1: 98 percent / acetonitrile / 20 h / 20 °C

2: sodium hydride / tetrahydrofuran / 65 °C

3: 94 percent / sodium azide; ammonium chloride / H₂O; 2-methoxy-ethanol / 3 h / 100 °C

4: 90 percent / pyridine / CH₂Cl₂ / cooling

5: 71 percent / triphenylphosphine / tetrahydrofuran / 1 h / 50 °C

With pyridine; sodium azide; ammonium chloride; sodium hydride; triphenylphosphine; In tetrahydrofuran; dichloromethane; 2-methoxy-ethanol; water; acetonitrile;
DOI:10.1016/j.tetasy.2006.06.009