(2S,3R)-3-azido-1,2-diphenyloxycarbonyloxy-3-(4-methylthiophenyl)-propane

Base Information

Chemical Name:(2S,3R)-3-azido-1,2-diphenyloxycarbonyloxy-3-(4-methylthiophenyl)-propane
CAS No.:909767-31-3
Molecular Formula:C₂₄H₂₁N₃O₆S
Molecular Weight:479.513
Hs Code.:

Synonyms:(2S,3R)-3-azido-1,2-diphenyloxycarbonyloxy-3-(4-methylthiophenyl)-propane

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Chemical Property of (2S,3R)-3-azido-1,2-diphenyloxycarbonyloxy-3-(4-methylthiophenyl)-propane

Chemical Property:

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Technology Process of (2S,3R)-3-azido-1,2-diphenyloxycarbonyloxy-3-(4-methylthiophenyl)-propane

There total 4 articles about (2S,3R)-3-azido-1,2-diphenyloxycarbonyloxy-3-(4-methylthiophenyl)-propane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 909767-30-2
(2S,3R)-3-azido-3-(4-methylthiophenyl)-1,2-propanediol

: 1885-14-9
phenyl chloroformate

: 909767-31-3
(2S,3R)-3-azido-1,2-diphenyloxycarbonyloxy-3-(4-methylthiophenyl)-propane

Guidance literature:: With pyridine; In dichloromethane; cooling;
DOI:10.1016/j.tetasy.2006.06.009

Reference yield:

: 909767-29-9
(2R,3S)-2,3-epoxy-3-(4-methylthiophenyl)-1-propanol

: 909767-31-3
(2S,3R)-3-azido-1,2-diphenyloxycarbonyloxy-3-(4-methylthiophenyl)-propane

Guidance literature:: Multi-step reaction with 2 steps

1: 94 percent / sodium azide; ammonium chloride / H₂O; 2-methoxy-ethanol / 3 h / 100 °C

2: 90 percent / pyridine / CH₂Cl₂ / cooling

With pyridine; sodium azide; ammonium chloride; In dichloromethane; 2-methoxy-ethanol; water;
DOI:10.1016/j.tetasy.2006.06.009

Reference yield:

: 906548-44-5
(1S,2S)-(+)-2-(dimethylamino)-1-[4-(methylthio)phenyl]propane-1,3-diol

: 909767-31-3
(2S,3R)-3-azido-1,2-diphenyloxycarbonyloxy-3-(4-methylthiophenyl)-propane

Guidance literature:: Multi-step reaction with 4 steps

1: 98 percent / acetonitrile / 20 h / 20 °C

2: sodium hydride / tetrahydrofuran / 65 °C

3: 94 percent / sodium azide; ammonium chloride / H₂O; 2-methoxy-ethanol / 3 h / 100 °C

4: 90 percent / pyridine / CH₂Cl₂ / cooling

With pyridine; sodium azide; ammonium chloride; sodium hydride; In tetrahydrofuran; dichloromethane; 2-methoxy-ethanol; water; acetonitrile;
DOI:10.1016/j.tetasy.2006.06.009