1-(2-azido-1-(4-(trifluoromethoxy)benzyloxy)ethyl)-2,4-dichlorobenzene

Base Information

Chemical Name:1-(2-azido-1-(4-(trifluoromethoxy)benzyloxy)ethyl)-2,4-dichlorobenzene
CAS No.:1301629-39-9
Molecular Formula:C₁₆H₁₂Cl₂F₃N₃O₂
Molecular Weight:406.191
Hs Code.:

Synonyms:1-(2-azido-1-(4-(trifluoromethoxy)benzyloxy)ethyl)-2,4-dichlorobenzene

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Chemical Property of 1-(2-azido-1-(4-(trifluoromethoxy)benzyloxy)ethyl)-2,4-dichlorobenzene

Chemical Property:

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Technology Process of 1-(2-azido-1-(4-(trifluoromethoxy)benzyloxy)ethyl)-2,4-dichlorobenzene

There total 2 articles about 1-(2-azido-1-(4-(trifluoromethoxy)benzyloxy)ethyl)-2,4-dichlorobenzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 1301629-37-7
2-azido-1-(2,4-dichlorophenyl)ethan-1-ol

: 50824-05-0
4-trifluoromethoxybenzyl bromide

: 1301629-39-9
1-(2-azido-1-(4-(trifluoromethoxy)benzyloxy)ethyl)-2,4-dichlorobenzene

Guidance literature:: With tetra-(n-butyl)ammonium iodide; sodium hydride; In N,N-dimethyl-formamide; mineral oil; at -78 - 20 ℃; Inert atmosphere;
DOI:10.1016/j.bmcl.2012.09.041

Reference yield:

: 13692-14-3,114446-57-0
α-(chloromethyl)-2,4-dichlorobenzyl alcohol

: 1301629-39-9
1-(2-azido-1-(4-(trifluoromethoxy)benzyloxy)ethyl)-2,4-dichlorobenzene

Guidance literature:: Multi-step reaction with 2 steps

1: sodium azide; tetra-(n-butyl)ammonium iodide / N,N-dimethyl-formamide / 12 h / Reflux

2: tetra-(n-butyl)ammonium iodide; sodium hydride / N,N-dimethyl-formamide; mineral oil / -78 - 20 °C / Inert atmosphere

With sodium azide; tetra-(n-butyl)ammonium iodide; sodium hydride; In N,N-dimethyl-formamide; mineral oil;
DOI:10.1016/j.bmcl.2012.09.041

Reference yield: 81.0%

: 1301629-39-9
1-(2-azido-1-(4-(trifluoromethoxy)benzyloxy)ethyl)-2,4-dichlorobenzene

: 927-74-2
3-Butyn-1-ol

: 1301628-97-6
2-(1-(2-(2,4-dichlorophenyl)-2-(4-(trifluoromethoxy)benzyloxy)ethyl)-1H-1,2,3-triazol-4-yl)ethanol

Guidance literature:: With copper(l) iodide; N-ethyl-N,N-diisopropylamine; In dichloromethane; at 150 ℃; for 0.166667h; Microwave irradiation;
DOI:10.1016/j.bmcl.2012.09.041