1-Methoxy-(1-phenylsulfanyl)-2-methyl-4-(3,4-methylenedioxyphenyl)butan-2-ol

Base Information

Chemical Name:1-Methoxy-(1-phenylsulfanyl)-2-methyl-4-(3,4-methylenedioxyphenyl)butan-2-ol
CAS No.:264875-14-1
Molecular Formula:C₁₉H₂₂O₄S
Molecular Weight:346.447
Hs Code.:

Synonyms:1-Methoxy-(1-phenylsulfanyl)-2-methyl-4-(3,4-methylenedioxyphenyl)butan-2-ol

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1-Methoxy-(1-phenylsulfanyl)-2-methyl-4-(3,4-methylenedioxyphenyl)butan-2-ol

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Technology Process of 1-Methoxy-(1-phenylsulfanyl)-2-methyl-4-(3,4-methylenedioxyphenyl)butan-2-ol

There total 1 articles about 1-Methoxy-(1-phenylsulfanyl)-2-methyl-4-(3,4-methylenedioxyphenyl)butan-2-ol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: 55418-52-5
cassione

: 13865-50-4
methoxymethyl phenyl sulfide

: 264875-14-1
1-Methoxy-(1-phenylsulfanyl)-2-methyl-4-(3,4-methylenedioxyphenyl)butan-2-ol

Guidance literature:: methoxymethyl phenyl sulfide; With n-butyllithium; In tetrahydrofuran; hexane; at -78 ℃; for 0.5h;

cassione; In tetrahydrofuran; hexane; at -78 ℃; for 0.333333h; Further stages.;

Reference yield: 70.0%

: 264875-14-1
1-Methoxy-(1-phenylsulfanyl)-2-methyl-4-(3,4-methylenedioxyphenyl)butan-2-ol

: 264875-15-2
2-Methyl-4-(3,4-methylenedioxyphenyl)-2-phenylsulfanylbutanal

Guidance literature:: With pyridine; thionyl chloride; In dichloromethane; at 0 ℃; for 0.75h;

Reference yield:

: 264875-14-1
1-Methoxy-(1-phenylsulfanyl)-2-methyl-4-(3,4-methylenedioxyphenyl)butan-2-ol

: 120749-42-0,120749-51-1
(2RS,3RS,4SR)-2,4-Dimethyl-2-[2-(3,4-methylenedioxyphenyl)ethyl]-3-phenylsulfanyltetrahydrofuran

Guidance literature:: Multi-step reaction with 4 steps

1.1: 70 percent / SOCl₂; pyridine / CH₂Cl₂ / 0.75 h / 0 °C

2.1: LDA / hexane; tetrahydrofuran / 0.5 h / -78 °C

2.2: 13 percent / hexane; tetrahydrofuran / 0.5 h / -78 °C

3.1: 76 percent / LiAlH₄ / diethyl ether / 3 h / 0 °C

4.1: 96 percent / p-TsOH / benzene / 0.08 h / Heating

With pyridine; lithium aluminium tetrahydride; thionyl chloride; toluene-4-sulfonic acid; lithium diisopropyl amide; In tetrahydrofuran; diethyl ether; hexane; dichloromethane; benzene; 1.1: Oxidation / 2.1: Metallation / 2.2: Addition / 3.1: Reduction / 4.1: Cyclization;