Methyl 4-[[[(1,1-dimethylethoxy)carbonyl]amino]carbonyl]benzoate

Base Information

Chemical Name:Methyl 4-[[[(1,1-dimethylethoxy)carbonyl]amino]carbonyl]benzoate
CAS No.:120158-08-9
Molecular Formula:C₁₄H₁₇NO₅
Molecular Weight:279.293
Hs Code.:
DSSTox Substance ID:DTXSID001172404

Synonyms:DTXSID001172404;Methyl 4-[[[(1,1-dimethylethoxy)carbonyl]amino]carbonyl]benzoate;120158-08-9

Suppliers and Price of Methyl 4-[[[(1,1-dimethylethoxy)carbonyl]amino]carbonyl]benzoate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Methyl 4-[[[(1,1-dimethylethoxy)carbonyl]amino]carbonyl]benzoate

Chemical Property:

XLogP3:2.2
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:5
Rotatable Bond Count:5
Exact Mass:279.11067264
Heavy Atom Count:20
Complexity:378

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:CC(C)(C)OC(=O)NC(=O)C1=CC=C(C=C1)C(=O)OC

Technology Process of Methyl 4-[[[(1,1-dimethylethoxy)carbonyl]amino]carbonyl]benzoate

There total 3 articles about Methyl 4-[[[(1,1-dimethylethoxy)carbonyl]amino]carbonyl]benzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 120157-96-2
methyl 4-[N-(tert-butoxycarbonyl)aminomethyl]benzoate

: 120158-08-9
methyl 4-((tert-butoxycarbonyl)carbamoyl)benzoate

Guidance literature:: With ruthenium(IV) oxide; sodium periodate; In ethyl acetate; for 2h; Ambient temperature;

Reference yield:

: 18469-52-8
methyl 4-(aminomethyl)benzoate

: 120158-08-9
methyl 4-((tert-butoxycarbonyl)carbamoyl)benzoate

Guidance literature:: Multi-step reaction with 2 steps

1: 94 percent / triethylamine / H₂O; dioxane / 6 h / Ambient temperature

2: 92 percent / ruthenium dioxide hydrate, 10percent aqueous NaIO₄ / ethyl acetate / 2 h / Ambient temperature

With ruthenium(IV) oxide; sodium periodate; triethylamine; In 1,4-dioxane; water; ethyl acetate;

Reference yield:

: 41840-28-2
S-tert-butoxycarbonyl-4,6-dimethyl-2-mercaptopyrimidine

: 120158-08-9
methyl 4-((tert-butoxycarbonyl)carbamoyl)benzoate

Guidance literature:: Multi-step reaction with 2 steps

1: 94 percent / triethylamine / H₂O; dioxane / 6 h / Ambient temperature

2: 92 percent / ruthenium dioxide hydrate, 10percent aqueous NaIO₄ / ethyl acetate / 2 h / Ambient temperature

With ruthenium(IV) oxide; sodium periodate; triethylamine; In 1,4-dioxane; water; ethyl acetate;