Technology Process of methyl 3-<(phenylsulfinyl)methyl>-1,4,8-trimethoxy-2-naphthoate
There total 9 articles about methyl 3-<(phenylsulfinyl)methyl>-1,4,8-trimethoxy-2-naphthoate which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
sodium periodate;
In
methanol; water;
for 72h;
Ambient temperature;
DOI:10.1021/jo01303a025
- Guidance literature:
-
Multi-step reaction with 7 steps
1: 9percent HCl / acetic acid / 12 h / Heating
2: 72 percent / p-toluenesulfonic acid / benzene / 3 h / Heating
3: 98 percent / 30percent H2O2 / acetic acid / 1) RT, 2) reflux; m-chloroperbenzoic acid
5: 84 percent / N-bromosuccinimide, benzoyl peroxide / Heating; Irradiation
6: 1) sodium ethoxide / 1) in EtOH, 10 min., 2) in THF, reflux overnight
7: 95 percent / NaIO4 / H2O; methanol / 72 h / Ambient temperature
With
hydrogenchloride; sodium periodate; N-Bromosuccinimide; Perbenzoic acid; dihydrogen peroxide; sodium ethanolate;
toluene-4-sulfonic acid;
In
methanol; water; acetic acid; benzene;
DOI:10.1021/jo01303a025
- Guidance literature:
-
Multi-step reaction with 6 steps
1: 72 percent / p-toluenesulfonic acid / benzene / 3 h / Heating
2: 98 percent / 30percent H2O2 / acetic acid / 1) RT, 2) reflux; m-chloroperbenzoic acid
4: 84 percent / N-bromosuccinimide, benzoyl peroxide / Heating; Irradiation
5: 1) sodium ethoxide / 1) in EtOH, 10 min., 2) in THF, reflux overnight
6: 95 percent / NaIO4 / H2O; methanol / 72 h / Ambient temperature
With
sodium periodate; N-Bromosuccinimide; Perbenzoic acid; dihydrogen peroxide; sodium ethanolate;
toluene-4-sulfonic acid;
In
methanol; water; acetic acid; benzene;
DOI:10.1021/jo01303a025
