O-benzoyl-N-(4-tert-butyldimethylsiloxy-2-methoxybenzyl)-N-(4-methoxyphenyl)glycolamide

Base Information

Chemical Name:O-benzoyl-N-(4-tert-butyldimethylsiloxy-2-methoxybenzyl)-N-(4-methoxyphenyl)glycolamide
CAS No.:1341219-68-8
Molecular Formula:C₃₀H₃₇NO₆Si
Molecular Weight:535.712
Hs Code.:

Synonyms:O-benzoyl-N-(4-tert-butyldimethylsiloxy-2-methoxybenzyl)-N-(4-methoxyphenyl)glycolamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of O-benzoyl-N-(4-tert-butyldimethylsiloxy-2-methoxybenzyl)-N-(4-methoxyphenyl)glycolamide

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Technology Process of O-benzoyl-N-(4-tert-butyldimethylsiloxy-2-methoxybenzyl)-N-(4-methoxyphenyl)glycolamide

There total 5 articles about O-benzoyl-N-(4-tert-butyldimethylsiloxy-2-methoxybenzyl)-N-(4-methoxyphenyl)glycolamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 1341219-49-5
N-(4-tert-butyldimethylsiloxy-2-methoxybenzyl)-p-anisidine

: 614-44-8
benzoyloxyacetic acid

: 1341219-68-8
O-benzoyl-N-(4-tert-butyldimethylsiloxy-2-methoxybenzyl)-N-(4-methoxyphenyl)glycolamide

Guidance literature:: With dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In dichloromethane; at 20 ℃; for 0.166667h;
DOI:10.1021/jo201495w

Reference yield:

: 129742-36-5
(4-((tert-butyldimethylsilyl)oxy)-2-methoxybenzaldehyde)

: 1341219-68-8
O-benzoyl-N-(4-tert-butyldimethylsiloxy-2-methoxybenzyl)-N-(4-methoxyphenyl)glycolamide

Guidance literature:: Multi-step reaction with 3 steps

1: acetic acid / dichloromethane / 0.17 h / 20 °C

2: sodium tris(acetoxy)borohydride / 0.33 h / 0 - 20 °C

3: dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 0.17 h / 20 °C

With dmap; sodium tris(acetoxy)borohydride; acetic acid; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In dichloromethane;
DOI:10.1021/jo201495w

Reference yield:

: C₂₁H₂₉NO₃Si

: 1341219-68-8
O-benzoyl-N-(4-tert-butyldimethylsiloxy-2-methoxybenzyl)-N-(4-methoxyphenyl)glycolamide

Guidance literature:: Multi-step reaction with 2 steps

1: sodium tris(acetoxy)borohydride / 0.33 h / 0 - 20 °C

2: dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 0.17 h / 20 °C

With dmap; sodium tris(acetoxy)borohydride; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In dichloromethane;
DOI:10.1021/jo201495w