4-oxo-octanoic acid [2-(tert-butyl-diphenyl-silanyloxy)-1-(3,4-dimethoxy-benzyl)-ethyl]-amide

Base Information

Chemical Name:4-oxo-octanoic acid [2-(tert-butyl-diphenyl-silanyloxy)-1-(3,4-dimethoxy-benzyl)-ethyl]-amide
CAS No.:862819-81-6
Molecular Formula:C₃₅H₄₇NO₅Si
Molecular Weight:589.847
Hs Code.:

4-oxo-octanoic acid [2-(<i>tert</i>-butyl-diphenyl-silanyloxy)-1-(3,4-dimethoxy-benzyl)-ethyl]-amide

Synonyms:4-oxo-octanoic acid [2-(tert-butyl-diphenyl-silanyloxy)-1-(3,4-dimethoxy-benzyl)-ethyl]-amide

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Chemical Property of 4-oxo-octanoic acid [2-(tert-butyl-diphenyl-silanyloxy)-1-(3,4-dimethoxy-benzyl)-ethyl]-amide

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Technology Process of 4-oxo-octanoic acid [2-(tert-butyl-diphenyl-silanyloxy)-1-(3,4-dimethoxy-benzyl)-ethyl]-amide

There total 7 articles about 4-oxo-octanoic acid [2-(tert-butyl-diphenyl-silanyloxy)-1-(3,4-dimethoxy-benzyl)-ethyl]-amide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 32161-30-1
(S)-3,4-dimethoxyphenylalanine

: 862819-81-6
4-oxo-octanoic acid [2-(tert-butyl-diphenyl-silanyloxy)-1-(3,4-dimethoxy-benzyl)-ethyl]-amide

Guidance literature:: Multi-step reaction with 7 steps

2.1: 92 percent

3.1: 87 percent / LiAlH₄

4.1: 95 percent

5.1: 86 percent / TFA

6.2: 75 percent / Ac₂O; NaOAc

7.1: tetrahydrofuran; diethyl ether / 6 h / -78 °C

With lithium aluminium tetrahydride; trifluoroacetic acid; In tetrahydrofuran; diethyl ether;
DOI:10.1016/S0040-4039(00)02319-4

Reference yield:

: 105779-71-3
(S)-(-)-[2-(3,4-dimethoxyphenyl)-1-hydroxymethylethyl]carbamic acid tert-butyl ester

: 862819-81-6
4-oxo-octanoic acid [2-(tert-butyl-diphenyl-silanyloxy)-1-(3,4-dimethoxy-benzyl)-ethyl]-amide

Guidance literature:: Multi-step reaction with 4 steps

1.1: 95 percent

2.1: 86 percent / TFA

3.2: 75 percent / Ac₂O; NaOAc

4.1: tetrahydrofuran; diethyl ether / 6 h / -78 °C

With trifluoroacetic acid; In tetrahydrofuran; diethyl ether;
DOI:10.1016/S0040-4039(00)02319-4

Reference yield:

: 138908-56-2
(S)-(+)-2-tert-butoxycarbonylamino-3-(3,4-dimethoxyphenyl)propionic acid methyl ester

: 862819-81-6
4-oxo-octanoic acid [2-(tert-butyl-diphenyl-silanyloxy)-1-(3,4-dimethoxy-benzyl)-ethyl]-amide

Guidance literature:: Multi-step reaction with 5 steps

1.1: 87 percent / LiAlH₄

2.1: 95 percent

3.1: 86 percent / TFA

4.2: 75 percent / Ac₂O; NaOAc

5.1: tetrahydrofuran; diethyl ether / 6 h / -78 °C

With lithium aluminium tetrahydride; trifluoroacetic acid; In tetrahydrofuran; diethyl ether;
DOI:10.1016/S0040-4039(00)02319-4