C₃₃H₃₂N₂O₉

Base Information

Chemical Name:C₃₃H₃₂N₂O₉
CAS No.:1287721-52-1
Molecular Formula:C₃₃H₃₂N₂O₉
Molecular Weight:600.625
Hs Code.:

C<sub>33</sub>H<sub>32</sub>N<sub>2</sub>O<sub>9</sub>

Synonyms:C₃₃H₃₂N₂O₉

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Chemical Property of C₃₃H₃₂N₂O₉

Chemical Property:

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Technology Process of C₃₃H₃₂N₂O₉

There total 6 articles about C₃₃H₃₂N₂O₉ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 67.0%

: 1287721-51-0
1-[2-O-acetyl-3-deoxy-3-carboxymethyl-5-O-(p-methoxytrityl)-pentofuranosyl]-uracil

: 1287721-52-1
C₃₃H₃₂N₂O₉

Guidance literature:: With sodium chlorite; sodium dihydrogenphosphate; water; In dimethyl sulfoxide; tert-butyl alcohol; at 20 ℃; for 30h; Inert atmosphere;
DOI:10.1002/anie.201007012

Reference yield:

: 1022902-92-6
1-[3-allyl-3-deoxy-pentofuranosyl]-uracil

: 1287721-52-1
C₃₃H₃₂N₂O₉

Guidance literature:: Multi-step reaction with 5 steps

1: pyridine / 0 - 20 °C / Inert atmosphere

2: pyridine; dmap / 4 h / 20 °C / Inert atmosphere

3: osmium(VIII) oxide; water; 4-methylmorpholine N-oxide / 1,4-dioxane / 10 h / 20 °C / Inert atmosphere

4: sodium periodate / 1,4-dioxane; water / 10 h / 20 °C / Inert atmosphere

5: sodium dihydrogenphosphate; sodium chlorite; water / dimethyl sulfoxide; tert-butyl alcohol / 30 h / 20 °C / Inert atmosphere

With pyridine; dmap; sodium chlorite; sodium periodate; sodium dihydrogenphosphate; osmium(VIII) oxide; water; 4-methylmorpholine N-oxide; In 1,4-dioxane; water; dimethyl sulfoxide; tert-butyl alcohol;
DOI:10.1002/anie.201007012

Reference yield:

: 200011-14-9
1-[3-C-allyl-2,5-O-bis(tert-butyldimethylsilyl)-β-D-pentofuranosyl]-uracyl

: 1287721-52-1
C₃₃H₃₂N₂O₉

Guidance literature:: Multi-step reaction with 6 steps

1: tetrabutyl ammonium fluoride / tetrahydrofuran / 24 h / 20 °C / Inert atmosphere

2: pyridine / 0 - 20 °C / Inert atmosphere

3: pyridine; dmap / 4 h / 20 °C / Inert atmosphere

4: osmium(VIII) oxide; water; 4-methylmorpholine N-oxide / 1,4-dioxane / 10 h / 20 °C / Inert atmosphere

5: sodium periodate / 1,4-dioxane; water / 10 h / 20 °C / Inert atmosphere

6: sodium dihydrogenphosphate; sodium chlorite; water / dimethyl sulfoxide; tert-butyl alcohol / 30 h / 20 °C / Inert atmosphere

With pyridine; dmap; sodium chlorite; sodium periodate; sodium dihydrogenphosphate; osmium(VIII) oxide; tetrabutyl ammonium fluoride; water; 4-methylmorpholine N-oxide; In tetrahydrofuran; 1,4-dioxane; water; dimethyl sulfoxide; tert-butyl alcohol;
DOI:10.1002/anie.201007012