3-benzyloxy-4-methoxy-ω-pyrrolidin-2-ylacetophenone

Base Information

Chemical Name:3-benzyloxy-4-methoxy-ω-pyrrolidin-2-ylacetophenone
CAS No.:77513-53-2
Molecular Formula:C₂₀H₂₃NO₃
Molecular Weight:325.408
Hs Code.:

Synonyms:3-benzyloxy-4-methoxy-ω-pyrrolidin-2-ylacetophenone

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Chemical Property of 3-benzyloxy-4-methoxy-ω-pyrrolidin-2-ylacetophenone

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Technology Process of 3-benzyloxy-4-methoxy-ω-pyrrolidin-2-ylacetophenone

There total 5 articles about 3-benzyloxy-4-methoxy-ω-pyrrolidin-2-ylacetophenone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: 77513-50-9
2-(3-benzyloxy-4-methoxybenzoyl)acetic acid

: 110-60-1
1,4-diaminobutane

: 77513-53-2
3-benzyloxy-4-methoxy-ω-pyrrolidin-2-ylacetophenone

Guidance literature:: In water; at 28 ℃; for 18h; catalase, pea seedling diamine oxidase (6.7 units), potassium phosphate buffer (0.2M), pH 7;

Reference yield: 50.0%

: 5724-81-2
1-pyrroline

: 77513-50-9
2-(3-benzyloxy-4-methoxybenzoyl)acetic acid

: 77513-53-2
3-benzyloxy-4-methoxy-ω-pyrrolidin-2-ylacetophenone

Guidance literature:: In methanol; water; for 48h; Ambient temperature; phosphate buffer, pH ca. 7.0;
DOI:10.1016/0040-4020(80)80227-4

Reference yield:

: 77513-52-1
ethyl 2-(3-benzyloxy-4-methoxybenzoyl)acetoacetate

: 77513-53-2
3-benzyloxy-4-methoxy-ω-pyrrolidin-2-ylacetophenone

Guidance literature:: Multi-step reaction with 3 steps

1: 60 percent

2: 80 percent / 2.5percent NaOH / H₂O / 72 h / Ambient temperature

3: 87 percent / H₂O / 18 h / 28 °C / catalase, pea seedling diamine oxidase (6.7 units), potassium phosphate buffer (0.2M), pH 7

With sodium hydroxide; In water;