Diamino-β-cumidinsaeure

Base Information

• Chemical Name: Diamino-β-cumidinsaeure
• CAS No.: 99069-08-6
• Molecular Formula: C₁₀H₁₂N₂O₄
• Molecular Weight: 224.216
• Mol file: 99069-08-6.mol

Synonyms:Diamino-β-cumidinsaeure

Chemical Property of Diamino-β-cumidinsaeure

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of Diamino-β-cumidinsaeure

There total 5 articles about Diamino-β-cumidinsaeure which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

Diamino-β-cumidinsaeure-dimethylester (100254-82-8) → Diamino-β-cumidinsaeure (99069-08-6)

Guidance literature:

With sodium hydroxide; In ethanol; Heating;

DOI:10.1002/hlca.19610440205

Reference yield:

2,5-bis(chloromethyl)-p-xylene (6298-72-2) → Diamino-β-cumidinsaeure (99069-08-6)

Guidance literature:

Multi-step reaction with 5 steps

1: aq. HNO₃, H₂SO₄ / CHCl₃ / 5 h / Ambient temperature

2: HNO₃, O₂ / Heating

3: diethyl ether; methanol

4: Zn, aq. AcOH

5: aq. NaOH / ethanol / Heating

With sodium hydroxide; sulfuric acid; oxygen; nitric acid; acetic acid; zinc; In methanol; diethyl ether; ethanol; chloroform;

DOI:10.1002/hlca.19610440205

Reference yield:

2,5-bis(chloromethyl)-3,6-dimethyl-1,4-dinitrobenzene (103905-76-6) → Diamino-β-cumidinsaeure (99069-08-6)

Guidance literature:

Multi-step reaction with 4 steps

1: HNO₃, O₂ / Heating

2: diethyl ether; methanol

3: Zn, aq. AcOH

4: aq. NaOH / ethanol / Heating

With sodium hydroxide; oxygen; nitric acid; acetic acid; zinc; In methanol; diethyl ether; ethanol;

DOI:10.1002/hlca.19610440205

upstream raw materials:

Diamino-β-cumidinsaeure-dimethylester

2,5-bis(chloromethyl)-p-xylene

2,5-bis(chloromethyl)-3,6-dimethyl-1,4-dinitrobenzene

Dinitro-β-cumidinsaeure

Downstream raw materials:

2,5-Dimethyl-1,4-phenylenediamine