3-{2-[3-(tert-butyl-dimethyl-silanyloxy)-propyl]-4-methoxy-phenyl}-prop-2-en-1-ol

Base Information

Chemical Name:3-{2-[3-(tert-butyl-dimethyl-silanyloxy)-propyl]-4-methoxy-phenyl}-prop-2-en-1-ol
CAS No.:853061-22-0
Molecular Formula:C₁₉H₃₂O₃Si
Molecular Weight:336.547
Hs Code.:

3-{2-[3-(<i>tert</i>-butyl-dimethyl-silanyloxy)-propyl]-4-methoxy-phenyl}-prop-2-en-1-ol

Synonyms:3-{2-[3-(tert-butyl-dimethyl-silanyloxy)-propyl]-4-methoxy-phenyl}-prop-2-en-1-ol

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Chemical Property of 3-{2-[3-(tert-butyl-dimethyl-silanyloxy)-propyl]-4-methoxy-phenyl}-prop-2-en-1-ol

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Technology Process of 3-{2-[3-(tert-butyl-dimethyl-silanyloxy)-propyl]-4-methoxy-phenyl}-prop-2-en-1-ol

There total 7 articles about 3-{2-[3-(tert-butyl-dimethyl-silanyloxy)-propyl]-4-methoxy-phenyl}-prop-2-en-1-ol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 853061-24-2
3-{2-[3-(tert-butyl-dimethyl-silanyloxy)-propyl]-4-methoxy-phenyl}-acrylic acid ethyl ester

: 853061-22-0
3-{2-[3-(tert-butyl-dimethyl-silanyloxy)-propyl]-4-methoxy-phenyl}-prop-2-en-1-ol

Guidance literature:: With diisobutylaluminium hydride; In dichloromethane; at 0 ℃; for 1h;
DOI:10.1139/v05-259

Reference yield:

: 853061-12-8
2-(3-hydroxy-propyl)-4-methoxy-benzaldehyde

: 853061-22-0
3-{2-[3-(tert-butyl-dimethyl-silanyloxy)-propyl]-4-methoxy-phenyl}-prop-2-en-1-ol

Guidance literature:: Multi-step reaction with 3 steps

1: 100 percent / imidazole / tetrahydrofuran / 0.75 h / 20 °C

2: 97 percent / sodium hydride / tetrahydrofuran / 0.33 h / 20 °C

3: 97 percent / diisobutylaluminium hydride / CH₂Cl₂ / 1 h / 0 °C

With 1H-imidazole; sodium hydride; diisobutylaluminium hydride; In tetrahydrofuran; dichloromethane; 2: Horner-Emmons reaction;
DOI:10.1139/v05-259

Reference yield:

: 853061-14-0
2-[3-(tert-butyl-dimethyl-silanyloxy)-propyl]-4-methoxy-benzaldehyde

: 853061-22-0
3-{2-[3-(tert-butyl-dimethyl-silanyloxy)-propyl]-4-methoxy-phenyl}-prop-2-en-1-ol

Guidance literature:: Multi-step reaction with 2 steps

1: 97 percent / sodium hydride / tetrahydrofuran / 0.33 h / 20 °C

2: 97 percent / diisobutylaluminium hydride / CH₂Cl₂ / 1 h / 0 °C

With sodium hydride; diisobutylaluminium hydride; In tetrahydrofuran; dichloromethane; 1: Horner-Emmons reaction;
DOI:10.1139/v05-259