(4S,5S)-kohlensaeure-<(5-benzyloxymethyl-2,2-dimethyl-1,3-dioxolan-4-yl)methyl>methylester

Base Information

Chemical Name:(4S,5S)-kohlensaeure-<(5-benzyloxymethyl-2,2-dimethyl-1,3-dioxolan-4-yl)methyl>methylester
CAS No.:78513-05-0
Molecular Formula:C₁₆H₂₂O₆
Molecular Weight:310.347
Hs Code.:

Synonyms:(4S,5S)-kohlensaeure-<(5-benzyloxymethyl-2,2-dimethyl-1,3-dioxolan-4-yl)methyl>methylester

Suppliers and Price of (4S,5S)-kohlensaeure-<(5-benzyloxymethyl-2,2-dimethyl-1,3-dioxolan-4-yl)methyl>methylester

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (4S,5S)-kohlensaeure-<(5-benzyloxymethyl-2,2-dimethyl-1,3-dioxolan-4-yl)methyl>methylester

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Technology Process of (4S,5S)-kohlensaeure-<(5-benzyloxymethyl-2,2-dimethyl-1,3-dioxolan-4-yl)methyl>methylester

There total 1 articles about (4S,5S)-kohlensaeure-<(5-benzyloxymethyl-2,2-dimethyl-1,3-dioxolan-4-yl)methyl>methylester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 78469-77-9,81076-11-1,128820-40-6,78513-03-8
(4S,5S)-4-benzyloxymethyl-5-hydroxymethyl-2,2-dimethyl-1,3-dioxolane

: 79-22-1
methyl chloroformate

: 78513-05-0
(4S,5S)-kohlensaeure-<(5-benzyloxymethyl-2,2-dimethyl-1,3-dioxolan-4-yl)methyl>methylester

Guidance literature:: With pyridine; In diethyl ether; 1.) 10 min., -20 deg C, 2.) room temp., overnight;
DOI:10.1002/hlca.19810640311

Reference yield:

: 78513-05-0
(4S,5S)-kohlensaeure-<(5-benzyloxymethyl-2,2-dimethyl-1,3-dioxolan-4-yl)methyl>methylester

: 78469-84-8
Carbonic acid (2S,3S)-4-benzyloxy-2,3-dihydroxy-butyl ester methyl ester

Guidance literature:: With toluene-4-sulfonic acid; In tetrahydrofuran; water; at 70 - 75 ℃; for 19h;
DOI:10.1002/hlca.19810640311

Reference yield:

: 78513-05-0
(4S,5S)-kohlensaeure-<(5-benzyloxymethyl-2,2-dimethyl-1,3-dioxolan-4-yl)methyl>methylester

: 78513-07-2
(-)-(2S,3R)-2,3-epoxy-4-(benzyloxy)-1-butanol

Guidance literature:: Multi-step reaction with 3 steps

1: p-toluenesulfonic acid monohydrate / tetrahydrofuran; H₂O / 19 h / 70 - 75 °C

2: 1.) CF₃COOH, 2.) pyridine / 1.) methylene dichloride, 15 h., reflux, 2.) 42 h., 22 deg C, methylene dichloride

3: 93 percent / 1N KOH / tetrahydrofuran; methanol / 2.5 h / Ambient temperature

With pyridine; potassium hydroxide; toluene-4-sulfonic acid; trifluoroacetic acid; In tetrahydrofuran; methanol; water;
DOI:10.1002/hlca.19810640311