Technology Process of C45H63N7O12S
There total 10 articles about C45H63N7O12S which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
benzotriazol-1-ol; O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; N-ethyl-N,N-diisopropylamine;
In
N,N-dimethyl-formamide;
at 20 ℃;
for 72h;
DOI:10.1039/b110453e
- Guidance literature:
-
With
benzotriazol-1-ol; O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; N-ethyl-N,N-diisopropylamine;
In
N,N-dimethyl-formamide;
at 20 ℃;
for 24h;
DOI:10.1039/b006192l
- Guidance literature:
-
Multi-step reaction with 8 steps
1: 75 percent / BF3*Et2O / acetonitrile / 1.5 h / 20 °C
2: 0.185 g / NIS / tetrahydrofuran / 144 h / 20 °C
3: 20 percent / tetrabutylammonium azide / 24 h / 70 °C
4: 95 percent / TFA / 0.75 h / 20 °C
5: 75 percent / NaOMe / methanol / 0.5 h / 20 °C
6: 72 percent / CrO3; aq. H2SO4 / acetone / 3 h / 20 °C
7: 47 percent / 2-(1H-benzotriazol-1-yl)-1,1,3,3-tetramethyluronium*PF6; HOBt; (i-Pr)2NEt / dimethylformamide / 72 h / 20 °C
With
chromium(VI) oxide; N-iodo-succinimide; sulfuric acid; boron trifluoride diethyl etherate; sodium methylate; tetrabutylammoniun azide; benzotriazol-1-ol; O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; N-ethyl-N,N-diisopropylamine; trifluoroacetic acid;
In
tetrahydrofuran; methanol; N,N-dimethyl-formamide; acetone; acetonitrile;
DOI:10.1039/b110453e