6-<<<2-(hydroxymethyl)phenyl>imino>methyl>-5-hydroxy-2,3-dihydrobenzofuran

Base Information

Chemical Name:6-<<<2-(hydroxymethyl)phenyl>imino>methyl>-5-hydroxy-2,3-dihydrobenzofuran
CAS No.:99385-90-7
Molecular Formula:C₁₆H₁₅NO₃
Molecular Weight:269.3
Hs Code.:

Synonyms:6-<<<2-(hydroxymethyl)phenyl>imino>methyl>-5-hydroxy-2,3-dihydrobenzofuran

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Chemical Property of 6-<<<2-(hydroxymethyl)phenyl>imino>methyl>-5-hydroxy-2,3-dihydrobenzofuran

Chemical Property:

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Technology Process of 6-<<<2-(hydroxymethyl)phenyl>imino>methyl>-5-hydroxy-2,3-dihydrobenzofuran

There total 6 articles about 6-<<<2-(hydroxymethyl)phenyl>imino>methyl>-5-hydroxy-2,3-dihydrobenzofuran which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 59.0%

: 5344-90-1
2-Aminobenzyl alcohol

: 99385-88-3
5-hydroxy-2,3-dihydrobenzofuran-6-carboxaldehyde

: 99385-90-7
6-<<<2-(hydroxymethyl)phenyl>imino>methyl>-5-hydroxy-2,3-dihydrobenzofuran

Guidance literature:: In methanol; Heating;

Reference yield:

: 39581-55-0
5-methoxy-benzofuran-3-one

: 99385-90-7
6-<<<2-(hydroxymethyl)phenyl>imino>methyl>-5-hydroxy-2,3-dihydrobenzofuran

Guidance literature:: Multi-step reaction with 4 steps

1: 99 percent / H₂ / 20percent palladium hydroxide / ethanol / 2280 Torr

2: 41 percent / TiCl₄ / CH₂Cl₂ / 1.5 h / Ambient temperature

3: 76 percent / BBr₃ / CH₂Cl₂ / 1.) -78 deg C, 15 min, 2.) from -78 deg C to RT, 2.5 h

4: 59 percent / methanol / Heating

With hydrogen; boron tribromide; titanium tetrachloride; palladium dihydroxide; In methanol; ethanol; dichloromethane;

Reference yield:

: 75717-53-2
2-chloro-1-(2-hydroxy-5-methoxyphenyl)ethan-1-one

: 99385-90-7
6-<<<2-(hydroxymethyl)phenyl>imino>methyl>-5-hydroxy-2,3-dihydrobenzofuran

Guidance literature:: Multi-step reaction with 5 steps

1: AcONa / methanol / 1.5 h / Heating

2: 99 percent / H₂ / 20percent palladium hydroxide / ethanol / 2280 Torr

3: 41 percent / TiCl₄ / CH₂Cl₂ / 1.5 h / Ambient temperature

4: 76 percent / BBr₃ / CH₂Cl₂ / 1.) -78 deg C, 15 min, 2.) from -78 deg C to RT, 2.5 h

5: 59 percent / methanol / Heating

With hydrogen; sodium acetate; boron tribromide; titanium tetrachloride; palladium dihydroxide; In methanol; ethanol; dichloromethane;