Ethanone, 2-chloro-1-(2-hydroxy-5-methoxyphenyl)-

Base Information

Chemical Name:Ethanone, 2-chloro-1-(2-hydroxy-5-methoxyphenyl)-
CAS No.:75717-53-2
Molecular Formula:C9H9ClO3
Molecular Weight:200.622
Hs Code.:

Synonyms:2-Chlor-1-(2-hydroxy-5-methoxy-phenyl)-aethanon;α-chloro-2-hydroxy-5-methoxyacetophenone;2-Hydroxy-5-methoxyphenacylchlorid;2-chloro-1-(2-hydroxy-5-methoxy-phenyl)-ethanone;

Suppliers and Price of Ethanone, 2-chloro-1-(2-hydroxy-5-methoxyphenyl)-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Alichem
2-Chloro-1-(2-hydroxy-5-methoxyphenyl)ethanone
5g
$ 660.33

Total 6 raw suppliers

Chemical Property of Ethanone, 2-chloro-1-(2-hydroxy-5-methoxyphenyl)-

Chemical Property:

Melting Point:83-84 °C
Boiling Point:317.3±27.0 °C(Predicted)
PSA：46.53000
Density:1.296±0.06 g/cm3(Predicted)
LogP:1.82230

Purity/Quality:

97% ^*data from raw suppliers

2-Chloro-1-(2-hydroxy-5-methoxyphenyl)ethanone ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of Ethanone, 2-chloro-1-(2-hydroxy-5-methoxyphenyl)-

There total 6 articles about Ethanone, 2-chloro-1-(2-hydroxy-5-methoxyphenyl)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.8%

: 1204-22-4
2-chloro-1-(2,5-dimethoxy-phenyl)-ethanone

: 75717-53-2
2-chloro-1-(2-hydroxy-5-methoxyphenyl)ethan-1-one

Guidance literature:: With aluminum (III) chloride; In dichloromethane; at 0 - 20 ℃; for 12h;
DOI:10.1021/acs.jmedchem.1c01411

Reference yield: 67.4%

: 107-14-2
chloroacetonitrile

: 150-76-5
4-methoxy-phenol

: 75717-53-2
2-chloro-1-(2-hydroxy-5-methoxyphenyl)ethan-1-one

: 123-31-9,8027-02-9
hydroquinone

Guidance literature:: With hydrogenchloride; aluminium trichloride; boron trichloride; Yield given. Multistep reaction; 1) 20 h, 1,2-dichloroethane, 2) 30 min;
DOI:10.1021/jo00314a046

Reference yield: 66.0%

: 59354-24-4
chloroacetonitrile

: 150-76-5
4-methoxy-phenol

: 75717-53-2
2-chloro-1-(2-hydroxy-5-methoxyphenyl)ethan-1-one

Guidance literature:: With aluminum (III) chloride; boron trichloride; In dichloromethane; at 0 - 25 ℃; for 6h; Inert atmosphere;
DOI:10.1016/j.ejmech.2017.02.048