hydroxy-4-(dihydroxy-2',4'-methyl-6'-benzoyl)-3-methoxy-6-dimethyl-2,5-benzoate de methyle

Base Information

• Chemical Name: hydroxy-4-(dihydroxy-2',4'-methyl-6'-benzoyl)-3-methoxy-6-dimethyl-2,5-benzoate de methyle
• CAS No.: 126717-87-1
• Molecular Formula: C₁₉H₂₀O₇
• Molecular Weight: 360.364

Synonyms:hydroxy-4-(dihydroxy-2',4'-methyl-6'-benzoyl)-3-methoxy-6-dimethyl-2,5-benzoate de methyle

Chemical Property of hydroxy-4-(dihydroxy-2',4'-methyl-6'-benzoyl)-3-methoxy-6-dimethyl-2,5-benzoate de methyle

Chemical Property:

Purity/Quality:

98% ^*data from raw suppliers

Safty Information:

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Technology Process of hydroxy-4-(dihydroxy-2',4'-methyl-6'-benzoyl)-3-methoxy-6-dimethyl-2,5-benzoate de methyle

There total 3 articles about hydroxy-4-(dihydroxy-2',4'-methyl-6'-benzoyl)-3-methoxy-6-dimethyl-2,5-benzoate de methyle which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

benzyloxy-4--3-methoxy-6-dimethyl-2,5-benzoate de methyle (126717-86-0) → hydroxy-4-(dihydroxy-2',4'-methyl-6'-benzoyl)-3-methoxy-6-dimethyl-2,5-benzoate de methyle (126717-87-1)

Guidance literature:

With hydrogenchloride; hydrogen; palladium on activated charcoal; In ethyl acetate;

DOI:10.1002/hlca.19890720524

Reference yield:

(((5-methyl-1,3-phenylene)bis(oxy))bis(methylene))dibenzene (36776-43-9) → hydroxy-4-(dihydroxy-2',4'-methyl-6'-benzoyl)-3-methoxy-6-dimethyl-2,5-benzoate de methyle (126717-87-1)

Guidance literature:

Multi-step reaction with 2 steps

1: 73 percent / (CF₃CO)2O / CH₂Cl₂ / 4 h / Ambient temperature

2: 87 percent / hydrogen, conc. HCl / 10percent Pd/C / ethyl acetate

With hydrogenchloride; hydrogen; trifluoroacetic anhydride; palladium on activated charcoal; In dichloromethane; ethyl acetate;

DOI:10.1002/hlca.19890720524

Reference yield:

2-benzyloxy-5-methoxycarbonyl-4-methoxy-3,6-dimethylbenzoic acid (78023-67-3) → hydroxy-4-(dihydroxy-2',4'-methyl-6'-benzoyl)-3-methoxy-6-dimethyl-2,5-benzoate de methyle (126717-87-1)

Guidance literature:

Multi-step reaction with 2 steps

1: 73 percent / (CF₃CO)2O / CH₂Cl₂ / 4 h / Ambient temperature

2: 87 percent / hydrogen, conc. HCl / 10percent Pd/C / ethyl acetate

With hydrogenchloride; hydrogen; trifluoroacetic anhydride; palladium on activated charcoal; In dichloromethane; ethyl acetate;

DOI:10.1002/hlca.19890720524

upstream raw materials:

benzyloxy-4--3-methoxy-6-dimethyl-2,5-benzoate de methyle

(((5-methyl-1,3-phenylene)bis(oxy))bis(methylene))dibenzene

2-benzyloxy-5-methoxycarbonyl-4-methoxy-3,6-dimethylbenzoic acid

Downstream raw materials:

acide -6-formyl-3-hydroxy-4-methyl-2-benzoique

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