methyl 2-(tert-butoxycarbonyl)-1,3,4,5-tetrahydro-2H-pyrido[4,3-b]indole-8-carboxylate

Base Information

Chemical Name:methyl 2-(tert-butoxycarbonyl)-1,3,4,5-tetrahydro-2H-pyrido[4,3-b]indole-8-carboxylate
CAS No.:1015082-05-9
Molecular Formula:C₁₈H₂₂N₂O₄
Molecular Weight:330.384
Hs Code.:

Synonyms:methyl 2-(tert-butoxycarbonyl)-1,3,4,5-tetrahydro-2H-pyrido[4,3-b]indole-8-carboxylate

Suppliers and Price of methyl 2-(tert-butoxycarbonyl)-1,3,4,5-tetrahydro-2H-pyrido[4,3-b]indole-8-carboxylate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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price

Chemenu
2-tert-Butyl8-methyl3,4-dihydro-1H-pyrido[4,3-b]indole-2,8(5H)-dicarboxylate 95%+
1g
$ 1587.00

American Custom Chemicals Corporation
2-TERT-BUTYL 8-METHYL 3,4-DIHYDRO-1H-PYRIDO-[4,3-B]-INDOLE-2,8-(5H)-DICARBOXYLATE 95.00%
5MG
$ 504.92

Total 2 raw suppliers

Chemical Property of methyl 2-(tert-butoxycarbonyl)-1,3,4,5-tetrahydro-2H-pyrido[4,3-b]indole-8-carboxylate

Chemical Property:

Purity/Quality:

99% ^*data from raw suppliers

2-tert-Butyl8-methyl3,4-dihydro-1H-pyrido[4,3-b]indole-2,8(5H)-dicarboxylate 95%+ ^*data from reagent suppliers

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Technology Process of methyl 2-(tert-butoxycarbonyl)-1,3,4,5-tetrahydro-2H-pyrido[4,3-b]indole-8-carboxylate

There total 2 articles about methyl 2-(tert-butoxycarbonyl)-1,3,4,5-tetrahydro-2H-pyrido[4,3-b]indole-8-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 1015082-04-8
methyl 2,3,4,5-tetrahydro-1H-pyrido[4,3-b]indole-8-carboxylate

: 1538-75-6
2,2-dimethylpropanoic anhydride

: 1015082-05-9
methyl 2-(tert-butoxycarbonyl)-1,3,4,5-tetrahydro-2H-pyrido[4,3-b]indole-8-carboxylate

Guidance literature:: With sodium hydroxide; In methanol; at 20 ℃; for 2.5h;

Reference yield: 100.0%

: 1015082-04-8
methyl 2,3,4,5-tetrahydro-1H-pyrido[4,3-b]indole-8-carboxylate

: 24424-99-5
di-tert-butyl dicarbonate

: 1015082-05-9
methyl 2-(tert-butoxycarbonyl)-1,3,4,5-tetrahydro-2H-pyrido[4,3-b]indole-8-carboxylate

Guidance literature:: With sodium hydroxide; In methanol; at 20 ℃; for 2.5h;

Reference yield: 66.0%

: 1015082-05-9
methyl 2-(tert-butoxycarbonyl)-1,3,4,5-tetrahydro-2H-pyrido[4,3-b]indole-8-carboxylate

: 100-52-7
benzaldehyde

: 1160786-83-3
methyl 2-benzyl-2,3,4,5-tetrahydro-1H-pyrido[4,3-b]indole-8-carboxylate

Guidance literature:: methyl 2-(tert-butoxycarbonyl)-1,3,4,5-tetrahydro-2H-pyrido[4,3-b]indole-8-carboxylate; With trifluoroacetic acid; In dichloromethane; at 20 ℃; for 1h;

benzaldehyde; With sodium tris(acetoxy)borohydride; acetic acid; In tetrahydrofuran; methanol; at 20 ℃;

With water; sodium hydrogencarbonate; In tetrahydrofuran; methanol; Product distribution / selectivity; Saturated solution;