(1R,5S,7R)-1,5,7-Tris-benzyloxymethyl-2,4-dioxo-3-aza-bicyclo[3.3.1]nonane-7-carboxylic acid anthracen-2-ylamide

Base Information

Chemical Name:(1R,5S,7R)-1,5,7-Tris-benzyloxymethyl-2,4-dioxo-3-aza-bicyclo[3.3.1]nonane-7-carboxylic acid anthracen-2-ylamide
CAS No.:146651-58-3
Molecular Formula:C₄₇H₄₄N₂O₆
Molecular Weight:732.876
Hs Code.:

Synonyms:(1R,5S,7R)-1,5,7-Tris-benzyloxymethyl-2,4-dioxo-3-aza-bicyclo[3.3.1]nonane-7-carboxylic acid anthracen-2-ylamide

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Chemical Property of (1R,5S,7R)-1,5,7-Tris-benzyloxymethyl-2,4-dioxo-3-aza-bicyclo[3.3.1]nonane-7-carboxylic acid anthracen-2-ylamide

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Technology Process of (1R,5S,7R)-1,5,7-Tris-benzyloxymethyl-2,4-dioxo-3-aza-bicyclo[3.3.1]nonane-7-carboxylic acid anthracen-2-ylamide

There total 7 articles about (1R,5S,7R)-1,5,7-Tris-benzyloxymethyl-2,4-dioxo-3-aza-bicyclo[3.3.1]nonane-7-carboxylic acid anthracen-2-ylamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 17690-16-3
benzyl bromomethyl ether

: 146651-58-3
(1R,5S,7R)-1,5,7-Tris-benzyloxymethyl-2,4-dioxo-3-aza-bicyclo[3.3.1]nonane-7-carboxylic acid anthracen-2-ylamide

Guidance literature:: Multi-step reaction with 6 steps

1: 1.) LDA

2: KOH / ethanol / Heating

3: xylene / Heating

4: aq. NH₃

5: SOCl₂

6: pyridine

With pyridine; potassium hydroxide; ammonium hydroxide; thionyl chloride; lithium diisopropyl amide; In ethanol; xylene;
DOI:10.1021/ja00055a066

Reference yield:

: 52831-11-5
trimethyl cyclohexane-1,3,5-tricarboxylate

: 146651-58-3
(1R,5S,7R)-1,5,7-Tris-benzyloxymethyl-2,4-dioxo-3-aza-bicyclo[3.3.1]nonane-7-carboxylic acid anthracen-2-ylamide

Guidance literature:: Multi-step reaction with 6 steps

1: 1.) LDA

2: KOH / ethanol / Heating

3: xylene / Heating

4: aq. NH₃

5: SOCl₂

6: pyridine

With pyridine; potassium hydroxide; ammonium hydroxide; thionyl chloride; lithium diisopropyl amide; In ethanol; xylene;
DOI:10.1021/ja00055a066

Reference yield:

: 146651-50-5
1,3,5-Tris-benzyloxymethyl-cyclohexane-1,3,5-tricarboxylic acid trimethyl ester

: 146651-58-3
(1R,5S,7R)-1,5,7-Tris-benzyloxymethyl-2,4-dioxo-3-aza-bicyclo[3.3.1]nonane-7-carboxylic acid anthracen-2-ylamide

Guidance literature:: Multi-step reaction with 5 steps

1: KOH / ethanol / Heating

2: xylene / Heating

3: aq. NH₃

4: SOCl₂

5: pyridine

With pyridine; potassium hydroxide; ammonium hydroxide; thionyl chloride; In ethanol; xylene;
DOI:10.1021/ja00055a066