Technology Process of C26H34O5
There total 5 articles about C26H34O5 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
18-crown-6 ether; potassium hexamethylsilazane;
In
tetrahydrofuran;
at 80 ℃;
for 24h;
DOI:10.1021/ol4003724
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: sodium hydride; tetra-(n-butyl)ammonium iodide / tetrahydrofuran / 0.17 h / 0 °C
1.2: 4.17 h / 0 - 80 °C / Inert atmosphere
2.1: tetrakis(triphenylphosphine) palladium(0) / toluene / 48 h / 100 °C / Inert atmosphere
3.1: cerium(III) chloride / tetrahydrofuran / 1.5 h / -78 °C
3.2: 5 h / -78 °C / Inert atmosphere
4.1: 18-crown-6 ether; potassium hexamethylsilazane / tetrahydrofuran / 24 h / 80 °C
With
tetrakis(triphenylphosphine) palladium(0); cerium(III) chloride; 18-crown-6 ether; tetra-(n-butyl)ammonium iodide; potassium hexamethylsilazane; sodium hydride;
In
tetrahydrofuran; toluene;
3.1: |Grignard Reaction / 3.2: |Grignard Reaction;
DOI:10.1021/ol4003724
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: tetrakis(triphenylphosphine) palladium(0) / toluene / 48 h / 100 °C / Inert atmosphere
2.1: cerium(III) chloride / tetrahydrofuran / 1.5 h / -78 °C
2.2: 5 h / -78 °C / Inert atmosphere
3.1: 18-crown-6 ether; potassium hexamethylsilazane / tetrahydrofuran / 24 h / 80 °C
With
tetrakis(triphenylphosphine) palladium(0); cerium(III) chloride; 18-crown-6 ether; potassium hexamethylsilazane;
In
tetrahydrofuran; toluene;
2.1: |Grignard Reaction / 2.2: |Grignard Reaction;
DOI:10.1021/ol4003724
