4-CHLORO-3-NITROBENZENESULFONOHYDRAZIDE

Base Information

• Chemical Name: 4-CHLORO-3-NITROBENZENESULFONOHYDRAZIDE
• CAS No.: 6655-80-7
• Molecular Formula: C6H6 Cl N3 O4 S
• Molecular Weight: 251.65
• Hs Code.: 2935009090
• Mol file: 6655-80-7.mol

Synonyms:4-Chloro-3-nitrobenzenesulfonohydrazide;4-Chloro-3-nitrophenylsulfonyl hydrazide

Chemical Property of 4-CHLORO-3-NITROBENZENESULFONOHYDRAZIDE

Chemical Property:

• Vapor Pressure: 5.27E-08mmHg at 25°C
• Boiling Point: 441.8°C at 760 mmHg
• Flash Point: 221°C
• PSA: 126.39000
• Density: 1.666g/cm³
• LogP: 3.09540

Purity/Quality:

97% ^*data from raw suppliers

4-Chloro-3-nitrobenzenesulfonohydrazide 97% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 4-CHLORO-3-NITROBENZENESULFONOHYDRAZIDE

There total 2 articles about 4-CHLORO-3-NITROBENZENESULFONOHYDRAZIDE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

3-nitro-4-chlorosulfonyl chloride (97-08-5) → 4-chloro-3-nitrobenzenesulfonylhydrazine (6655-80-7)

Guidance literature:

With hydrazine hydrate;

DOI:10.1039/j39660001229

Reference yield:

→ 4-chloro-3-nitrobenzenesulfonylhydrazine (6655-80-7)

Guidance literature:

4-Chlor-3-nitro-benzolsulfonylchlorid, N2H4*H2O;

Reference yield: 93.0%

4-chloro-3-nitrobenzenesulfonylhydrazine (6655-80-7) + ethyl acrylate (140-88-5,9003-32-1) → 3-[(4-chloro-3-nitrophenyl)sulfonyl]propanoic acid ethyl ester

Guidance literature:

In water; at 65 ℃; for 24h; Green chemistry;

DOI:10.1039/c4gc00932k

upstream raw materials:

3-nitro-4-chlorosulfonyl chloride

Downstream raw materials:

4-chloro-3-nitrobenzenesulfonyl fluoride

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