1,3-dimethyl-8-{[2-phenyl-2-oxoethyl]thio}-3,7-dihydro-1H-purine-2,6-dione

Base Information

Chemical Name:1,3-dimethyl-8-{[2-phenyl-2-oxoethyl]thio}-3,7-dihydro-1H-purine-2,6-dione
CAS No.:39140-87-9
Molecular Formula:C₁₅H₁₄N₄O₃S
Molecular Weight:330.367
Hs Code.:

Synonyms:1,3-dimethyl-8-{[2-phenyl-2-oxoethyl]thio}-3,7-dihydro-1H-purine-2,6-dione

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1,3-dimethyl-8-{[2-phenyl-2-oxoethyl]thio}-3,7-dihydro-1H-purine-2,6-dione

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Technology Process of 1,3-dimethyl-8-{[2-phenyl-2-oxoethyl]thio}-3,7-dihydro-1H-purine-2,6-dione

There total 6 articles about 1,3-dimethyl-8-{[2-phenyl-2-oxoethyl]thio}-3,7-dihydro-1H-purine-2,6-dione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 70-11-1
α-bromoacetophenone

: 1784-70-9
8-mercapto-1,3-dimethyl-1H-purine-2,6-(3H,7H)-dione

: 39140-87-9
1,3-dimethyl-8-{[2-phenyl-2-oxoethyl]thio}-3,7-dihydro-1H-purine-2,6-dione

Guidance literature:: With sodium hydroxide; In ethanol; water; at 20 ℃; for 4h;
DOI:10.1016/j.ejmech.2019.05.015

Reference yield:

: 39615-79-7
1-(2-cyanoacetyl)-1,3-dimethyl-urea

: 39140-87-9
1,3-dimethyl-8-{[2-phenyl-2-oxoethyl]thio}-3,7-dihydro-1H-purine-2,6-dione

Guidance literature:: Multi-step reaction with 5 steps

1: sodium hydroxide

2: sodium nitrite; acetic acid / water

3: ammonium hydroxide; sodium dithionite

4: N,N-dimethyl-formamide / 5 h / Reflux

5: sodium hydroxide / ethanol; water / 4 h / 20 °C

With ammonium hydroxide; sodium dithionite; acetic acid; sodium hydroxide; sodium nitrite; In ethanol; water; N,N-dimethyl-formamide;
DOI:10.1016/j.ejmech.2019.05.015

Reference yield:

: 6642-31-5
6-Amino-1,3-dimethylbarbituric acid

: 39140-87-9
1,3-dimethyl-8-{[2-phenyl-2-oxoethyl]thio}-3,7-dihydro-1H-purine-2,6-dione

Guidance literature:: Multi-step reaction with 4 steps

1: sodium nitrite; acetic acid / water

2: ammonium hydroxide; sodium dithionite

3: N,N-dimethyl-formamide / 5 h / Reflux

4: sodium hydroxide / ethanol; water / 4 h / 20 °C

With ammonium hydroxide; sodium dithionite; acetic acid; sodium hydroxide; sodium nitrite; In ethanol; water; N,N-dimethyl-formamide;
DOI:10.1016/j.ejmech.2019.05.015