methyl (1R,3R,4S,5R)-5-azido-3-benzoyloxy-1-benzyloxy-4-(methylsulfonyloxy)-cyclohexane-1-carboxylate-1,4-lactam

Base Information

Chemical Name:methyl (1R,3R,4S,5R)-5-azido-3-benzoyloxy-1-benzyloxy-4-(methylsulfonyloxy)-cyclohexane-1-carboxylate-1,4-lactam
CAS No.:1257059-80-5
Molecular Formula:C₂₃H₂₅N₃O₈S
Molecular Weight:503.533
Hs Code.:

Synonyms:methyl (1R,3R,4S,5R)-5-azido-3-benzoyloxy-1-benzyloxy-4-(methylsulfonyloxy)-cyclohexane-1-carboxylate-1,4-lactam

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Chemical Property of methyl (1R,3R,4S,5R)-5-azido-3-benzoyloxy-1-benzyloxy-4-(methylsulfonyloxy)-cyclohexane-1-carboxylate-1,4-lactam

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Technology Process of methyl (1R,3R,4S,5R)-5-azido-3-benzoyloxy-1-benzyloxy-4-(methylsulfonyloxy)-cyclohexane-1-carboxylate-1,4-lactam

There total 1 articles about methyl (1R,3R,4S,5R)-5-azido-3-benzoyloxy-1-benzyloxy-4-(methylsulfonyloxy)-cyclohexane-1-carboxylate-1,4-lactam which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 1257059-79-2
methyl (1R,3R,4S,5R)-5-azido-3-benzoyloxy-1-benzyloxy-4-hydroxy-cyclohexane-1-carboxylate

: 124-63-0
methanesulfonyl chloride

: 1257059-80-5
methyl (1R,3R,4S,5R)-5-azido-3-benzoyloxy-1-benzyloxy-4-(methylsulfonyloxy)-cyclohexane-1-carboxylate-1,4-lactam

Guidance literature:: With triethylamine; In dichloromethane; at 0 - 20 ℃; for 4h; Inert atmosphere;
DOI:10.1016/j.bmc.2010.08.027

Reference yield:

: 1257059-80-5
methyl (1R,3R,4S,5R)-5-azido-3-benzoyloxy-1-benzyloxy-4-(methylsulfonyloxy)-cyclohexane-1-carboxylate-1,4-lactam

: 1257059-81-6
methyl (1R,3R,4R,5R)-4,5-aziridino-3-benzoyloxy-1-benzyloxy-cyclohexane-1-carboxylate

Guidance literature:: methyl (1R,3R,4S,5R)-5-azido-3-benzoyloxy-1-benzyloxy-4-(methylsulfonyloxy)-cyclohexane-1-carboxylate-1,4-lactam; With triphenylphosphine; In tetrahydrofuran; at 0 - 20 ℃;

With water; triethylamine; In tetrahydrofuran; at 20 ℃; for 16h;
DOI:10.1016/j.bmc.2010.08.027