9H-fluorene-9-methanol, 9-(1-methylethyl)-

Base Information Edit

Chemical Name:9H-fluorene-9-methanol, 9-(1-methylethyl)-
CAS No.:97634-15-6
Molecular Formula:C₁₇H₁₈O
Molecular Weight:238.329
Hs Code.:
Mol file:97634-15-6.mol

Synonyms:9-isopropyl-9-(hydroxymethyl)fluorene

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 9H-fluorene-9-methanol, 9-(1-methylethyl)- Edit

Chemical Property:

Vapor Pressure:0mmHg at 25°C

Purity/Quality:

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Technology Process of 9H-fluorene-9-methanol, 9-(1-methylethyl)-

There total 6 articles about 9H-fluorene-9-methanol, 9-(1-methylethyl)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 97634-14-5
ethyl (9-isopropylfluoren-9-yl)carboxylate

: 97634-15-6
9-isopropyl-9-(hydroxymethyl)fluorene

Guidance literature:: With lithium aluminium tetrahydride; In diethyl ether; for 5h; Heating;
DOI:10.1021/jm00149a014

Reference yield: 86.0%

: 50-00-0,30525-89-4,61233-19-0
formaldehyd

: 3299-99-8
9-isopropyl-9H-fluorene

: 97634-15-6
9-isopropyl-9-(hydroxymethyl)fluorene

Guidance literature:: 9-isopropyl-9H-fluorene; With n-butyllithium; diisopropylamine; In tetrahydrofuran; hexane; at -5 ℃; for 0.5h;

formaldehyd; In tetrahydrofuran; hexane; at 25 ℃; Further stages.;
DOI:10.1021/jo8008897

Reference yield:

: 97634-16-7
9-isopropyl-9H-fluorene-9-carbaldehyde

: 3299-99-8
9-isopropyl-9H-fluorene

: 97634-15-6
9-isopropyl-9-(hydroxymethyl)fluorene

Guidance literature:: With lithium methanolate; (1,3-dioxolan-2-yl-methyl)triphenylphosphonium bromide; In methanol; N,N-dimethyl-formamide; at 80 ℃; for 24h;