3-(3,5-dimethylphenyl)-1-propanesulfonyl azide

Base Information

Chemical Name:3-(3,5-dimethylphenyl)-1-propanesulfonyl azide
CAS No.:90220-23-8
Molecular Formula:C₁₁H₁₅N₃O₂S
Molecular Weight:253.325
Hs Code.:

Synonyms:3-(3,5-dimethylphenyl)-1-propanesulfonyl azide

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Chemical Property of 3-(3,5-dimethylphenyl)-1-propanesulfonyl azide

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Technology Process of 3-(3,5-dimethylphenyl)-1-propanesulfonyl azide

There total 3 articles about 3-(3,5-dimethylphenyl)-1-propanesulfonyl azide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.3%

: 90220-70-5
3-(3,5-Dimethyl-phenyl)-propane-1-sulfonyl chloride

: 90220-23-8
3-(3,5-dimethylphenyl)-1-propanesulfonyl azide

Guidance literature:: With sodium azide; In water; acetone;
DOI:10.1021/jo00191a014

Reference yield:

: 90220-57-8
1-bromo-3-(3,5-dimethylphenyl)propane

: 90220-23-8
3-(3,5-dimethylphenyl)-1-propanesulfonyl azide

Guidance literature:: Multi-step reaction with 3 steps

1: Na₂SO₃

2: SOCl₂

3: 75.3 percent / NaN₃ / acetone; H₂O

With thionyl chloride; sodium azide; sodium sulfite; In water; acetone;
DOI:10.1021/jo00191a014

Reference yield:

: 90220-59-0
Sodium; 3-(3,5-dimethyl-phenyl)-propane-1-sulfonate

: 90220-23-8
3-(3,5-dimethylphenyl)-1-propanesulfonyl azide

Guidance literature:: Multi-step reaction with 2 steps

1: SOCl₂

2: 75.3 percent / NaN₃ / acetone; H₂O

With thionyl chloride; sodium azide; In water; acetone;
DOI:10.1021/jo00191a014