10-methylcarbonyloxy-1-(2,3,4,5-tetramethoxy-6-methylphenyl)decylacetate

Base Information

Chemical Name:10-methylcarbonyloxy-1-(2,3,4,5-tetramethoxy-6-methylphenyl)decylacetate
CAS No.:374622-18-1
Molecular Formula:C₂₅H₄₀O₈
Molecular Weight:468.588
Hs Code.:

Synonyms:10-methylcarbonyloxy-1-(2,3,4,5-tetramethoxy-6-methylphenyl)decylacetate

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Chemical Property of 10-methylcarbonyloxy-1-(2,3,4,5-tetramethoxy-6-methylphenyl)decylacetate

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Technology Process of 10-methylcarbonyloxy-1-(2,3,4,5-tetramethoxy-6-methylphenyl)decylacetate

There total 4 articles about 10-methylcarbonyloxy-1-(2,3,4,5-tetramethoxy-6-methylphenyl)decylacetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 108-24-7
acetic anhydride

: 374622-25-0
1-(2,3,4,5-tetramethoxy-6-methylphenyl)-1,10-decenediol

: 374622-18-1
10-methylcarbonyloxy-1-(2,3,4,5-tetramethoxy-6-methylphenyl)decylacetate

Guidance literature:: With dmap; triethylamine; In dichloromethane; at 20 ℃; for 7h;
DOI:10.1081/SCC-100105319

Reference yield:

: 14065-32-8
methyl 10-chloro-10-oxodecanoate

: 374622-18-1
10-methylcarbonyloxy-1-(2,3,4,5-tetramethoxy-6-methylphenyl)decylacetate

Guidance literature:: Multi-step reaction with 3 steps

1: 71 percent / AlCl₃ / CH₂Cl₂ / 24 h / Heating

2: 92 percent / LiAlH₄ / tetrahydrofuran / 1 h / 0 °C

3: 96 percent / Et₃N; DMAP / CH₂Cl₂ / 7 h / 20 °C

With dmap; lithium aluminium tetrahydride; aluminium trichloride; triethylamine; In tetrahydrofuran; dichloromethane; 1: Friedel-Crafts reaction;
DOI:10.1081/SCC-100105319

Reference yield:

: 818-88-2
sebacic acid mono methyl ester

: 374622-18-1
10-methylcarbonyloxy-1-(2,3,4,5-tetramethoxy-6-methylphenyl)decylacetate

Guidance literature:: Multi-step reaction with 4 steps

1: thionyl chloride

2: 71 percent / AlCl₃ / CH₂Cl₂ / 24 h / Heating

3: 92 percent / LiAlH₄ / tetrahydrofuran / 1 h / 0 °C

4: 96 percent / Et₃N; DMAP / CH₂Cl₂ / 7 h / 20 °C

With dmap; lithium aluminium tetrahydride; aluminium trichloride; thionyl chloride; triethylamine; In tetrahydrofuran; dichloromethane; 2: Friedel-Crafts reaction;
DOI:10.1081/SCC-100105319