2-{[5-(4-chlorophenyl)-4-iodo-1-phenyl-1H-pyrazol-3-yl]methyl}acrylonitrile

Base Information

Chemical Name:2-{[5-(4-chlorophenyl)-4-iodo-1-phenyl-1H-pyrazol-3-yl]methyl}acrylonitrile
CAS No.:1214996-39-0
Molecular Formula:C₁₉H₁₃ClIN₃
Molecular Weight:445.69
Hs Code.:

Synonyms:2-{[5-(4-chlorophenyl)-4-iodo-1-phenyl-1H-pyrazol-3-yl]methyl}acrylonitrile

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Chemical Property of 2-{[5-(4-chlorophenyl)-4-iodo-1-phenyl-1H-pyrazol-3-yl]methyl}acrylonitrile

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Technology Process of 2-{[5-(4-chlorophenyl)-4-iodo-1-phenyl-1H-pyrazol-3-yl]methyl}acrylonitrile

There total 1 articles about 2-{[5-(4-chlorophenyl)-4-iodo-1-phenyl-1H-pyrazol-3-yl]methyl}acrylonitrile which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 1214996-36-7
1-[5-(4-chlorophenyl)-4-iodo-1-phenyl-1H-pyrazol-3-yl]-2-cyanoallyl acetate

: 1214996-39-0
2-{[5-(4-chlorophenyl)-4-iodo-1-phenyl-1H-pyrazol-3-yl]methyl}acrylonitrile

Guidance literature:: 1-[5-(4-chlorophenyl)-4-iodo-1-phenyl-1H-pyrazol-3-yl]-2-cyanoallyl acetate; With 1,4-diaza-bicyclo[2.2.2]octane; In tetrahydrofuran; water; at 20 ℃; for 0.25h;

With sodium tetrahydroborate; In tetrahydrofuran; water; at 5 - 20 ℃;
DOI:10.1002/adsc.200900438

Reference yield: 86.0%

: 1214996-39-0
2-{[5-(4-chlorophenyl)-4-iodo-1-phenyl-1H-pyrazol-3-yl]methyl}acrylonitrile

: 1214996-42-5
2-{[5-(4-chlorophenyl)-4-iodo-1-phenyl-1H-pyrazol-3-yl]methyl}acrylamide

Guidance literature:: With sulfuric acid; trifluoroacetic acid; at 20 ℃; for 4h;
DOI:10.1002/adsc.200900438

Reference yield: 75.0%

: 1214996-39-0
2-{[5-(4-chlorophenyl)-4-iodo-1-phenyl-1H-pyrazol-3-yl]methyl}acrylonitrile

: 40138-16-7
2-formylbenzene boronic acid

: 1435483-31-0
2-{[5-(4-chlorophenyl)-4-(2-formylphenyl)-1-phenyl-1H-pyrazol-3-yl]methyl}prop-2-enenitrile

Guidance literature:: With tetrakis(triphenylphosphine) palladium⁽⁰⁾; sodium carbonate; In N,N-dimethyl-formamide; at 90 ℃; for 3h; Inert atmosphere;
DOI:10.1016/j.tet.2013.03.099