Dipropyl pyridine-2,6-dicarboxylate

Base Information

Chemical Name:Dipropyl pyridine-2,6-dicarboxylate
CAS No.:63597-03-5
Molecular Formula:C13H17 N O4
Molecular Weight:251.282
Hs Code.:
NSC Number:78917
DSSTox Substance ID:DTXSID50291885
Nikkaji Number:J737.142J
Wikidata:Q82029967

Synonyms:63597-03-5;dipropyl pyridine-2,6-dicarboxylate;NSC78917;SCHEMBL8405218;DTXSID50291885;NSC-78917

Suppliers and Price of Dipropyl pyridine-2,6-dicarboxylate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 5 raw suppliers

Chemical Property of Dipropyl pyridine-2,6-dicarboxylate

Chemical Property:

Vapor Pressure:8.62E-06mmHg at 25°C
Boiling Point:374°C at 760 mmHg
Flash Point:180°C
Density:1.119g/cm³
XLogP3:3
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:5
Rotatable Bond Count:8
Exact Mass:251.11575802
Heavy Atom Count:18
Complexity:254

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CCCOC(=O)C1=NC(=CC=C1)C(=O)OCCC

Technology Process of Dipropyl pyridine-2,6-dicarboxylate

There total 4 articles about Dipropyl pyridine-2,6-dicarboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 67.0%

: 71-23-8
propan-1-ol

: 3739-94-4
2,6-Pyridinedicarbonyl dichloride

: 1339960-93-8
2-(n-propoxycarbonyl)-pyridine-6-carboxylic acid

: 63597-03-5
di(n-propyl) pyridine-2,6-dicarboxylate

Guidance literature:: With N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; for 4h; Reflux;
DOI:10.1016/j.tet.2011.09.006

Reference yield:

: 499-83-2
Pyridine-2,6-dicarboxylic acid

: 1339960-93-8
2-(n-propoxycarbonyl)-pyridine-6-carboxylic acid

: 63597-03-5
di(n-propyl) pyridine-2,6-dicarboxylate

Guidance literature:: Multi-step reaction with 2 steps

1: thionyl chloride / 3 h / Reflux

2: N-ethyl-N,N-diisopropylamine / tetrahydrofuran / 4 h / Reflux

With thionyl chloride; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran;
DOI:10.1016/j.tet.2011.09.006