2-Amino-N-[2-(2-chloro-benzoyl)-4-nitro-phenyl]-N-methyl-acetamide; hydrobromide

Base Information

Chemical Name:2-Amino-N-[2-(2-chloro-benzoyl)-4-nitro-phenyl]-N-methyl-acetamide; hydrobromide
CAS No.:76337-75-2
Molecular Formula:BrH*C₁₆H₁₄ClN₃O₄
Molecular Weight:428.67
Hs Code.:

Synonyms:2-Amino-N-[2-(2-chloro-benzoyl)-4-nitro-phenyl]-N-methyl-acetamide; hydrobromide

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Chemical Property of 2-Amino-N-[2-(2-chloro-benzoyl)-4-nitro-phenyl]-N-methyl-acetamide; hydrobromide

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Technology Process of 2-Amino-N-[2-(2-chloro-benzoyl)-4-nitro-phenyl]-N-methyl-acetamide; hydrobromide

There total 2 articles about 2-Amino-N-[2-(2-chloro-benzoyl)-4-nitro-phenyl]-N-methyl-acetamide; hydrobromide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 76337-83-2
({[2-(2-Chloro-benzoyl)-4-nitro-phenyl]-methyl-carbamoyl}-methyl)-carbamic acid benzyl ester

: 76337-75-2
2-Amino-N-[2-(2-chloro-benzoyl)-4-nitro-phenyl]-N-methyl-acetamide; hydrobromide

Guidance literature:: With hydrogen bromide; In acetic acid; for 1h; Ambient temperature;
DOI:10.1021/jm00133a006

Reference yield:

: 76337-80-9
{[2-(2-Chloro-benzoyl)-4-nitro-phenylcarbamoyl]-methyl}-carbamic acid benzyl ester

: 76337-75-2
2-Amino-N-[2-(2-chloro-benzoyl)-4-nitro-phenyl]-N-methyl-acetamide; hydrobromide

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) NaH / 1.) DMF, oil, 2-5 deg C, 15 min, 2.) DMF, oil, 2-5 deg C, 2 h

2: 100 percent / 20percent HBr / acetic acid / 1 h / Ambient temperature

With hydrogen bromide; sodium hydride; In acetic acid;
DOI:10.1021/jm00133a006

Reference yield:

: 76337-75-2
2-Amino-N-[2-(2-chloro-benzoyl)-4-nitro-phenyl]-N-methyl-acetamide; hydrobromide

: 76337-76-3
2-(o-chlorobenzoyl)-4-nitro-N-methyl-N^α-glycylglycinanilide

Guidance literature:: Multi-step reaction with 2 steps

1: hexamethylphosphoric acid triamide; acetonitrile / 5 h / Ambient temperature

2: 34 percent / 30percent HBr / acetic acid / 2 h / Ambient temperature

With hydrogen bromide; In N,N,N,N,N,N-hexamethylphosphoric triamide; acetic acid; acetonitrile;
DOI:10.1021/jm00133a006