({[2-(2-Chloro-benzoyl)-4-nitro-phenyl]-methyl-carbamoyl}-methyl)-carbamic acid benzyl ester

Base Information

Chemical Name:({[2-(2-Chloro-benzoyl)-4-nitro-phenyl]-methyl-carbamoyl}-methyl)-carbamic acid benzyl ester
CAS No.:76337-83-2
Molecular Formula:C₂₄H₂₀ClN₃O₆
Molecular Weight:481.892
Hs Code.:

Synonyms:({[2-(2-Chloro-benzoyl)-4-nitro-phenyl]-methyl-carbamoyl}-methyl)-carbamic acid benzyl ester

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Chemical Property of ({[2-(2-Chloro-benzoyl)-4-nitro-phenyl]-methyl-carbamoyl}-methyl)-carbamic acid benzyl ester

Chemical Property:

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Technology Process of ({[2-(2-Chloro-benzoyl)-4-nitro-phenyl]-methyl-carbamoyl}-methyl)-carbamic acid benzyl ester

There total 1 articles about ({[2-(2-Chloro-benzoyl)-4-nitro-phenyl]-methyl-carbamoyl}-methyl)-carbamic acid benzyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 76337-80-9
{[2-(2-Chloro-benzoyl)-4-nitro-phenylcarbamoyl]-methyl}-carbamic acid benzyl ester

: 74-88-4
methyl iodide

: 76337-83-2
({[2-(2-Chloro-benzoyl)-4-nitro-phenyl]-methyl-carbamoyl}-methyl)-carbamic acid benzyl ester

Guidance literature:: With sodium hydride; Yield given. Multistep reaction; 1.) DMF, oil, 2-5 deg C, 15 min, 2.) DMF, oil, 2-5 deg C, 2 h;
DOI:10.1021/jm00133a006

Reference yield: 100.0%

: 76337-83-2
({[2-(2-Chloro-benzoyl)-4-nitro-phenyl]-methyl-carbamoyl}-methyl)-carbamic acid benzyl ester

: 76337-75-2
2-Amino-N-[2-(2-chloro-benzoyl)-4-nitro-phenyl]-N-methyl-acetamide; hydrobromide

Guidance literature:: With hydrogen bromide; In acetic acid; for 1h; Ambient temperature;
DOI:10.1021/jm00133a006

Reference yield:

: 76337-83-2
({[2-(2-Chloro-benzoyl)-4-nitro-phenyl]-methyl-carbamoyl}-methyl)-carbamic acid benzyl ester

: 76337-76-3
2-(o-chlorobenzoyl)-4-nitro-N-methyl-N^α-glycylglycinanilide

Guidance literature:: Multi-step reaction with 3 steps

1: 100 percent / 20percent HBr / acetic acid / 1 h / Ambient temperature

2: hexamethylphosphoric acid triamide; acetonitrile / 5 h / Ambient temperature

3: 34 percent / 30percent HBr / acetic acid / 2 h / Ambient temperature

With hydrogen bromide; In N,N,N,N,N,N-hexamethylphosphoric triamide; acetic acid; acetonitrile;
DOI:10.1021/jm00133a006