1-formyl-o-carborane tosylhydrazone

Base Information

• Chemical Name: 1-formyl-o-carborane tosylhydrazone
• CAS No.: 80737-45-7
• Molecular Formula: C₁₀H₂₀B₁₀N₂O₂S
• Molecular Weight: 340.457

Synonyms:1-formyl-o-carborane tosylhydrazone

Chemical Property of 1-formyl-o-carborane tosylhydrazone

Chemical Property:

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Technology Process of 1-formyl-o-carborane tosylhydrazone

There total 1 articles about 1-formyl-o-carborane tosylhydrazone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

1-formyl-o-carborane (20394-07-4) → 1-formyl-o-carborane tosylhydrazone (80737-45-7)

Guidance literature:

With hydrogenchloride; In methanol; underN2 or Ar, to soln. of 1-formyl-o-carborane in methanol added tosylhydrazine, 2 drops of concd. HCl added as catalyst, refluxed for 5 h; hot distd. water added, crystd. on cooling, recrystd. from methanol; elem. anal.;

DOI:10.1021/ja00375a033

upstream raw materials:

1-formyl-o-carborane

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