5-benzyl-4-(furan-2-yl)-2-phenylthiazole

Base Information

Chemical Name:5-benzyl-4-(furan-2-yl)-2-phenylthiazole
CAS No.:1259389-24-6
Molecular Formula:C₂₀H₁₅NOS
Molecular Weight:317.411
Hs Code.:

Synonyms:5-benzyl-4-(furan-2-yl)-2-phenylthiazole

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Chemical Property of 5-benzyl-4-(furan-2-yl)-2-phenylthiazole

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Technology Process of 5-benzyl-4-(furan-2-yl)-2-phenylthiazole

There total 3 articles about 5-benzyl-4-(furan-2-yl)-2-phenylthiazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 100-44-7
benzyl chloride

: 21036-63-5
4-(2-furyl)-2-phenylthiazole

: 1259389-24-6
5-benzyl-4-(furan-2-yl)-2-phenylthiazole

Guidance literature:: With palladium diacetate; potassium carbonate; triphenylphosphine; Trimethylacetic acid; In toluene; at 110 ℃; regioselective reaction; Inert atmosphere;
DOI:10.1021/jo102081a

Reference yield: 40.0%

: 1192-62-7,80145-44-4
1-(2-furyl)-1-ethanone

: 100-52-7
benzaldehyde

: 1259389-24-6
5-benzyl-4-(furan-2-yl)-2-phenylthiazole

Guidance literature:: With sulfur; ammonium iodide; In pyridine; water; at 150 ℃; for 20h; chemoselective reaction; Inert atmosphere; Sealed tube;
DOI:10.1039/c8gc03895c

Reference yield:

: 1192-62-7,80145-44-4
1-(2-furyl)-1-ethanone

: 1259389-24-6
5-benzyl-4-(furan-2-yl)-2-phenylthiazole

Guidance literature:: Multi-step reaction with 3 steps

1: copper(ll) bromide / ethyl acetate / Reflux

2: tetrahydrofuran / Reflux

3: palladium diacetate; potassium carbonate; triphenylphosphine; Trimethylacetic acid / toluene / 110 °C / Inert atmosphere

With palladium diacetate; potassium carbonate; triphenylphosphine; copper(ll) bromide; Trimethylacetic acid; In tetrahydrofuran; ethyl acetate; toluene;
DOI:10.1021/jo102081a