C₆₃H₈₄Cl₃N₅O₁₃S

Base Information

Chemical Name:C₆₃H₈₄Cl₃N₅O₁₃S
CAS No.:1075710-29-0
Molecular Formula:C₆₃H₈₄Cl₃N₅O₁₃S
Molecular Weight:1257.81
Hs Code.:

C<sub>63</sub>H<sub>84</sub>Cl<sub>3</sub>N<sub>5</sub>O<sub>13</sub>S

Synonyms:C₆₃H₈₄Cl₃N₅O₁₃S

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Chemical Property of C₆₃H₈₄Cl₃N₅O₁₃S

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Technology Process of C₆₃H₈₄Cl₃N₅O₁₃S

There total 13 articles about C₆₃H₈₄Cl₃N₅O₁₃S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 1352449-18-3
C₄₅H₆₉Cl₃N₄O₁₀S

: 35661-38-2,35661-39-3,79990-15-1,136132-75-7
N-(9-fluorenylmethoxycarbonyl)-D-alanine

: 1075710-29-0
C₆₃H₈₄Cl₃N₅O₁₃S

Guidance literature:: With dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In dichloromethane; at 0 - 20 ℃; for 6h;
DOI:10.1016/j.tet.2011.10.094

Reference yield:

: 20312-37-2,498-36-2
(R)-2-hydroxy-4-methylpentanoic acid

: 1075710-29-0
C₆₃H₈₄Cl₃N₅O₁₃S

Guidance literature:: Multi-step reaction with 4 steps

1: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine / N,N-dimethyl-formamide / 17 h / 20 °C

2: dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 22 h / 20 °C

3: pyridine; pyridine hydrogenfluoride / tetrahydrofuran / 12 h / 40 °C

4: dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 6 h / 0 - 20 °C

With pyridine; dmap; benzotriazol-1-ol; pyridine hydrogenfluoride; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1016/j.tet.2011.10.094

Reference yield:

: 1204215-22-4
C₈H₁₄Cl₃NO₂*ClH

: 1075710-29-0
C₆₃H₈₄Cl₃N₅O₁₃S

Guidance literature:: Multi-step reaction with 10 steps

1: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine / dichloromethane; N,N-dimethyl-formamide / 6 h / 20 °C

2: hydrogenchloride / 1,4-dioxane / 1 h / 10 - 15 °C

3: O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; N-ethyl-N,N-diisopropylamine / dichloromethane; N,N-dimethyl-formamide / 12 h / 20 °C

4: hydrogenchloride / 1,4-dioxane / 1 h / 0 °C

5: O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; triethylamine; N-ethyl-N,N-diisopropylamine / dichloromethane; N,N-dimethyl-formamide / 14 h / 20 °C

6: hydrogenchloride / 1,4-dioxane / 2 h / 20 °C

7: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine / N,N-dimethyl-formamide / 17 h / 20 °C

8: dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 22 h / 20 °C

9: pyridine; pyridine hydrogenfluoride / tetrahydrofuran / 12 h / 40 °C

10: dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 6 h / 0 - 20 °C

With pyridine; hydrogenchloride; dmap; benzotriazol-1-ol; O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; pyridine hydrogenfluoride; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; 1,4-dioxane; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1016/j.tet.2011.10.094