α-(ethyloxycarbonylamino)benzyl-2-(ethyloxycarbonyl)ethylphosphinic acid

Base Information

Chemical Name:α-(ethyloxycarbonylamino)benzyl-2-(ethyloxycarbonyl)ethylphosphinic acid
CAS No.:1029774-18-2
Molecular Formula:C₁₅H₂₂NO₆P
Molecular Weight:343.317
Hs Code.:

Synonyms:α-(ethyloxycarbonylamino)benzyl-2-(ethyloxycarbonyl)ethylphosphinic acid

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Chemical Property of α-(ethyloxycarbonylamino)benzyl-2-(ethyloxycarbonyl)ethylphosphinic acid

Chemical Property:

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Technology Process of α-(ethyloxycarbonylamino)benzyl-2-(ethyloxycarbonyl)ethylphosphinic acid

There total 3 articles about α-(ethyloxycarbonylamino)benzyl-2-(ethyloxycarbonyl)ethylphosphinic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 59.0%

: 3693-54-7
diethyl N,N'-benzylidenebis(carbamate)

: 126588-79-2
3-hydroxyphosphinoyl-propionic acid ethyl ester

: 1029774-18-2
α-(ethyloxycarbonylamino)benzyl-2-(ethyloxycarbonyl)ethylphosphinic acid

Guidance literature:: With trifluoroacetic anhydride; at 20 ℃;
DOI:10.1016/j.tetlet.2012.01.094

Reference yield:

: 126588-79-2
3-hydroxyphosphinoyl-propionic acid ethyl ester

: 100-52-7
benzaldehyde

: 51-79-6
urethane

: 1029774-18-2
α-(ethyloxycarbonylamino)benzyl-2-(ethyloxycarbonyl)ethylphosphinic acid

: 3693-54-7
diethyl N,N'-benzylidenebis(carbamate)

Guidance literature:: With acetyl chloride; In acetic anhydride; at 20 ℃; for 0.5h;
DOI:10.1016/j.tetlet.2010.03.020

Reference yield:

: 100-52-7
benzaldehyde

: 1029774-18-2
α-(ethyloxycarbonylamino)benzyl-2-(ethyloxycarbonyl)ethylphosphinic acid

Guidance literature:: Multi-step reaction with 2 steps

1: acetic anhydride

2: trifluoroacetic anhydride / 20 °C

With acetic anhydride; trifluoroacetic anhydride;
DOI:10.1134/S1070363213100150