Technology Process of C19H14INO6
There total 4 articles about C19H14INO6 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
ammonium cerium (IV) nitrate; caesium carbonate;
In
tetrahydrofuran;
at 60 ℃;
for 17h;
Inert atmosphere;
DOI:10.1021/ol203390w
- Guidance literature:
-
Multi-step reaction with 5 steps
1: 1,8-diazabicyclo[5.4.0]undec-7-ene / dichloromethane / 24 h / 23 °C / Inert atmosphere
2: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 0 °C / Inert atmosphere
3: benzene / 15 h / 100 °C / sealed tube; Inert atmosphere
4: pyridine; dmap; iodine / dichloromethane / 0.42 h / 0 °C / Inert atmosphere
5: ammonium cerium (IV) nitrate; caesium carbonate / tetrahydrofuran / 17 h / 60 °C / Inert atmosphere
With
pyridine; dmap; ammonium cerium (IV) nitrate; iodine; caesium carbonate; 1,8-diazabicyclo[5.4.0]undec-7-ene; 3-chloro-benzenecarboperoxoic acid;
In
tetrahydrofuran; dichloromethane; benzene;
DOI:10.1021/ol203390w
- Guidance literature:
-
Multi-step reaction with 3 steps
1: benzene / 15 h / 100 °C / sealed tube; Inert atmosphere
2: pyridine; dmap; iodine / dichloromethane / 0.42 h / 0 °C / Inert atmosphere
3: ammonium cerium (IV) nitrate; caesium carbonate / tetrahydrofuran / 17 h / 60 °C / Inert atmosphere
With
pyridine; dmap; ammonium cerium (IV) nitrate; iodine; caesium carbonate;
In
tetrahydrofuran; dichloromethane; benzene;
DOI:10.1021/ol203390w
