Ethyl 3-nitronaphthalene-2-carboxylate

Base Information

Chemical Name:Ethyl 3-nitronaphthalene-2-carboxylate
CAS No.:77802-23-4
Molecular Formula:C₁₃H₁₁NO₄
Molecular Weight:245.235
Hs Code.:2916399090
DSSTox Substance ID:DTXSID20506478
Wikidata:Q82362237
Mol file:77802-23-4.mol

Synonyms:77802-23-4;ETHYL 3-NITRO-2-NAPHTHOATE;Ethyl 3-nitronaphthalene-2-carboxylate;ETHYL3-NITRO-2-NAPHTHOATE;SCHEMBL5256338;DTXSID20506478

Suppliers and Price of Ethyl 3-nitronaphthalene-2-carboxylate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

American Custom Chemicals Corporation
ETHYL-3-NITRO-2-NAPHTHOATE 95.00%
5MG
$ 504.14

Total 5 raw suppliers

Chemical Property of Ethyl 3-nitronaphthalene-2-carboxylate

Chemical Property:

PSA：72.12000
LogP:3.44790
XLogP3:3.2
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:3
Exact Mass:245.06880783
Heavy Atom Count:18
Complexity:325

Purity/Quality:

98% ^*data from raw suppliers

ETHYL-3-NITRO-2-NAPHTHOATE 95.00% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CCOC(=O)C1=CC2=CC=CC=C2C=C1[N+](=O)[O-]

Technology Process of Ethyl 3-nitronaphthalene-2-carboxylate

There total 1 articles about Ethyl 3-nitronaphthalene-2-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 44.0%

: 3590-37-2
ethyl 3-nitropropanoate

: 643-79-8
o-phthalic dicarboxaldehyde

: 77802-23-4
3-Nitro-2-naphthoesaeure-aethylester

Guidance literature:: With sodium ethanolate; In ethanol; at 25 ℃; for 16h;
DOI:10.1021/ol0400443

Reference yield: 92.0%

: 77802-23-4
3-Nitro-2-naphthoesaeure-aethylester

: 73428-03-2
3-Nitro-2-naphthoesaeure

Guidance literature:: With sodium hydroxide; In ethanol; at 25 ℃; for 12h;
DOI:10.1021/ol0400443

Reference yield:

: 77802-23-4
3-Nitro-2-naphthoesaeure-aethylester

: 73428-04-3
(3-nitronaphthalen-2-yl)methanol

Guidance literature:: Multi-step reaction with 2 steps

1: 92 percent / aq. NaOH / ethanol / 12 h / 25 °C

2: 78 percent / B₂H₆ / dimethylsulfoxide / 12 h / 25 °C

With sodium hydroxide; diborane; In ethanol; dimethyl sulfoxide;
DOI:10.1021/ol0400443