C₂₈H₂₉FN₂O₂

Base Information

Chemical Name:C₂₈H₂₉FN₂O₂
CAS No.:1374108-69-6
Molecular Formula:C₂₈H₂₉FN₂O₂
Molecular Weight:444.549
Hs Code.:

C<sub>28</sub>H<sub>29</sub>FN<sub>2</sub>O<sub>2</sub>

Synonyms:C₂₈H₂₉FN₂O₂

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Chemical Property of C₂₈H₂₉FN₂O₂

Chemical Property:

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Technology Process of C₂₈H₂₉FN₂O₂

There total 6 articles about C₂₈H₂₉FN₂O₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 1374108-68-5
C₂₆H₂₅FN₂O₂

: 75-07-0,9002-91-9
acetaldehyde

: 1374108-69-6
C₂₈H₂₉FN₂O₂

Guidance literature:: With 2-picoline borane complex; acetic acid; In methanol; at 20 ℃; for 32h;

Reference yield:

: 112482-36-7
1-fluoro-3-(phenylmethoxy)propan-2-ol

: 1374108-69-6
C₂₈H₂₉FN₂O₂

Guidance literature:: Multi-step reaction with 5 steps

1: triphenylphosphine; di-isopropyl azodicarboxylate / tetrahydrofuran / 22 h / 20 °C / Cooling with ice

2: 2,6-di-tert-butyl-4-methylpyridine / dichloromethane / 2.5 h / 20 °C / Cooling with ice

3: tetrakis(triphenylphosphine) palladium⁽⁰⁾; sodium carbonate / water; 1,2-dimethoxyethane / 1.5 h / 90 °C / Inert atmosphere

4: trifluoroacetic acid / dichloromethane / 16 h / 20 °C / Cooling with ice

5: acetic acid; 2-picoline borane complex / methanol / 32 h / 20 °C

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; 2,6-di-tert-butyl-4-methylpyridine; 2-picoline borane complex; di-isopropyl azodicarboxylate; sodium carbonate; acetic acid; triphenylphosphine; trifluoroacetic acid; In tetrahydrofuran; methanol; 1,2-dimethoxyethane; dichloromethane; water;

Reference yield:

: 70500-72-0
quinoline-2,7-diol

: 1374108-69-6
C₂₈H₂₉FN₂O₂

Guidance literature:: Multi-step reaction with 5 steps

1: triphenylphosphine; di-isopropyl azodicarboxylate / tetrahydrofuran / 22 h / 20 °C / Cooling with ice

2: 2,6-di-tert-butyl-4-methylpyridine / dichloromethane / 2.5 h / 20 °C / Cooling with ice

3: tetrakis(triphenylphosphine) palladium⁽⁰⁾; sodium carbonate / water; 1,2-dimethoxyethane / 1.5 h / 90 °C / Inert atmosphere

4: trifluoroacetic acid / dichloromethane / 16 h / 20 °C / Cooling with ice

5: acetic acid; 2-picoline borane complex / methanol / 32 h / 20 °C

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; 2,6-di-tert-butyl-4-methylpyridine; 2-picoline borane complex; di-isopropyl azodicarboxylate; sodium carbonate; acetic acid; triphenylphosphine; trifluoroacetic acid; In tetrahydrofuran; methanol; 1,2-dimethoxyethane; dichloromethane; water;