C₃₄H₃₄O₁₂

Base Information

Chemical Name:C₃₄H₃₄O₁₂
CAS No.:1400055-66-4
Molecular Formula:C₃₄H₃₄O₁₂
Molecular Weight:634.637
Hs Code.:

C<sub>34</sub>H<sub>34</sub>O<sub>12</sub>

Synonyms:C₃₄H₃₄O₁₂

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Chemical Property of C₃₄H₃₄O₁₂

Chemical Property:

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Technology Process of C₃₄H₃₄O₁₂

There total 10 articles about C₃₄H₃₄O₁₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1400055-53-9
C₁₉H₁₈O₆

: 1283147-52-3
(R)-3-(3,4-dimethoxyphenyl)-1-methoxy-1-oxopropan-2-yl acrylate

: 1400055-66-4
C₃₄H₃₄O₁₂

Guidance literature:: With (2S,3S)-N-acetyl-2-amino-3-methylpentanoic acid; oxygen; palladium diacetate; potassium hydrogencarbonate; In tert-Amyl alcohol; at 85 ℃; for 6h;
DOI:10.1021/ol302273r DOI:10.1021/ol302273r

Reference yield:

: 54814-41-4,54640-00-5,54910-31-5
3-(3,4-dimethoxy-phenyl)-2-hydroxy-propionic acid methyl ester

: 1400055-66-4
C₃₄H₃₄O₁₂

Guidance literature:: Multi-step reaction with 2 steps

1: triethylamine; dmap / dichloromethane / 49 h / 0 - 23 °C

2: palladium diacetate; (2S,3S)-N-acetyl-2-amino-3-methylpentanoic acid; potassium hydrogencarbonate; oxygen / tert-Amyl alcohol / 6 h / 85 °C

With dmap; (2S,3S)-N-acetyl-2-amino-3-methylpentanoic acid; oxygen; palladium diacetate; potassium hydrogencarbonate; triethylamine; In tert-Amyl alcohol; dichloromethane;
DOI:10.1021/ol302273r DOI:10.1021/ol302273r

Reference yield:

: 74003-55-7
3,4-dibromobenzaldehyde

: 1400055-66-4
C₃₄H₃₄O₁₂

Guidance literature:: Multi-step reaction with 7 steps

1.1: piperdinium acetate / benzene / 6 h / Reflux

2.1: 9-O-benzylcupreidine / toluene / 48 h / 23 °C / Reflux

2.2: 2 h / 80 °C

3.1: bis-[(trifluoroacetoxy)iodo]benzene; formic acid; sulfuric acid / 12 h / 23 °C / Cooling with ice; Inert atmosphere

4.1: [1,3-bis(2,6-diisopropylphenyl)imidazol-2-ylidene](3-chloropyridyl) palladium(II) dichloride; triethylamine / 110 °C

5.1: sodium hydroxide; dihydrogen peroxide / tetrahydrofuran / 0.5 h / 0 °C / Inert atmosphere

5.2: 48 h / 55 °C / Inert atmosphere

6.1: barium hydroxide monohydrate / methanol; tetrahydrofuran / 23 °C

7.1: palladium diacetate; (2S,3S)-N-acetyl-2-amino-3-methylpentanoic acid; potassium hydrogencarbonate; oxygen / tert-Amyl alcohol / 6 h / 85 °C

With 9-O-benzylcupreidine; formic acid; [1,3-bis(2,6-diisopropylphenyl)imidazol-2-ylidene](3-chloropyridyl) palladium(II) dichloride; barium hydroxide monohydrate; (2S,3S)-N-acetyl-2-amino-3-methylpentanoic acid; sulfuric acid; dihydrogen peroxide; oxygen; palladium diacetate; piperdinium acetate; potassium hydrogencarbonate; triethylamine; bis-[(trifluoroacetoxy)iodo]benzene; sodium hydroxide; In tetrahydrofuran; methanol; tert-Amyl alcohol; toluene; benzene; 1.1: |Knoevenagel Condensation;
DOI:10.1021/ol302273r DOI:10.1021/ol302273r